2,3-二甲基-1,3-丁二烯合成路线 （共 777 条）
反应条件
1: 180 °C 2: phosphorus (V)-oxide / 330 °C View Scheme
参考文献
Skwartschenko et al.
Zhurnal Obshchei Khimii, 1955 , vol. 25, p. 1094,1095; engl. Ausg. S. 1051
参考文献
Journal of the American Chemical Society, , vol. 108, p. 2742
反应条件
in diethyl ether T=5°C; 48 h; Yield given. Yields of byproduct given;
参考文献
Gaumont; Wazneh; Denis
Tetrahedron, 1991 , vol. 47, # 27 p. 4927 - 4940
反应条件
T=82°C; Hydrogenation;
参考文献
Musaew
Doklady Akademii Nauk SSSR, 1951 , vol. 80, p. 759
Chem.Abstr., 1952 , p. 4463
反应条件
hydrogen; palladium dichloride in N,N-dimethyl-formamide P=18751.5 Torr; 0.25 h; Ambient temperaturevarious time; Product distribution;
参考文献
Acta Chimica Academiae Scientiarum Hungaricae, , vol. 103, # 1 p. 33 - 42
反应条件
[Ir(6-Neo)(COD)Cl] in ethanol P=3750.38 Torr; 1 h;
参考文献
Dunsford, Jay J.; Tromp, Dorette S.; Cavell, Kingsley J.; Elsevier, Cornelis J.; Kariuki, Benson M.
Dalton Transactions, 2013 , vol. 42, # 20 p. 7318 - 7329
反应条件
T=22°C; Hydrogenation;
参考文献
Gostunskaja et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 863,865; engl.Ausg.S.779,780,782
反应条件
in neat (no solvent) Irradiation (UV/VIS); Ge deriv. and a large excess of organic reagent irradiating in a quartztube for 4 h then concg. in vacuo; identified by high-pressure chromy. and NMR spectra;
参考文献
Riviere, P.; Castel, A.; Satge, J.; Guyot, D.
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 193 - 206
参考文献
Riviere, P.; Castel, A.; Satge, J.; Guyot, D.
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 193 - 206
反应条件
1.1: SOCl2; pyridine / benzene / 1.5 h / 20 °C 1.2: benzene / 5 h / Heating 2.1: 11.4 g / KOH / methanol / 2 h / Heating View Scheme
参考文献
D'Auria, Maurizio; De Luca, Eliana; Mauriello, Giacomo; Racioppi, Rocco; Sleiter, Giancarlo
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 16 p. 2369 - 2373
