2,3-二甲基-1,3-丁二烯合成路线 （共 777 条）
反应条件
sodium methylate; propionic acid 1.) room temp., 0.5 h, 2.) MeOH, 3.) reflux, 2 h; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Zaidlewicz, Marek; Binkul, Jacek R.; Sokol, Wojciech
Journal of Organometallic Chemistry, 1999 , vol. 580, # 2 p. 354 - 362
反应条件
sodium hydroxide 1.) 80 deg C, 6 h, 2.) ethylene glycol, 140 to 200 deg C, 0.5 h; Yield givenMultistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Zaidlewicz, Marek; Binkul, Jacek R.; Sokol, Wojciech
Journal of Organometallic Chemistry, 1999 , vol. 580, # 2 p. 354 - 362
反应条件
propionic acid 1.) 80 deg C, 6 h, 2.) reflux, 4 h; various reagents in 2nd step; Product distribution;
参考文献
Zaidlewicz, Marek; Binkul, Jacek R.; Sokol, Wojciech
Journal of Organometallic Chemistry, 1999 , vol. 580, # 2 p. 354 - 362
参考文献
House,H.O. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 1463 - 1466
反应条件
1,2,3-benzenetriol T=165°C;
参考文献
Gault; Laloi
Bulletin de la Societe Chimique de France, 1952 , p. 1079
反应条件
Yield given. Yields of byproduct given;
参考文献
Lambert, Joseph B.; Marko, Dale E.
Journal of the American Chemical Society, 1985 , vol. 107, # 26 p. 7978 - 7982
参考文献
Bolm, Carsten; Schiffers, Ingo; Dinter, Christian L.; Gerlach, Arne
Journal of Organic Chemistry, 2000 , vol. 65, # 21 p. 6984 - 6991
反应条件
1: toluene / 150 - 160 °C 2: aqueous KOH 3: acetic acid anhydride View Scheme
参考文献
Petrow; Sopow
Sb. Statei Obshch. Khim., 1953 , p. 853,855
Chem.Abstr., 1955 , p. 5329
参考文献
Craig
Journal of the American Chemical Society, 1951 , vol. 73, p. 4889,4891
反应条件
1: 2,3-dimethyl-buta-1,3-diene With lithium in tetrahydrofuran T=0 - 20°C; Inert atmosphere; 2: chloro-trimethyl-silane in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Aouf, Chahinez; El Abed, Douniazad; Giorgi, Michel; Santelli, Maurice
Tetrahedron, 2009 , vol. 65, # 28 p. 5563 - 5570
