2,3-二甲基-1,3-丁二烯合成路线 （共 777 条）
反应条件
in cyclohexane 24 h; Heating;
参考文献
Butler, Richard N.; O'Halloran, Gerard A.; Burke, Luke A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1855 - 1860
反应条件
2,2'-azo-bisisobutyronitrile 75°C;;
参考文献
Neumann, W. P.; Sommer, R.
Angewandte Chemie, 1964 , vol. 76, p. 52 - 53
Full Text Show Details
Neumann, W. P.; Sommer, R.
Liebigs Annalen der Chemie, 1967 , vol. 701, p. 28 - 39
反应条件
in neat (no solvent) Ge deriv. heating with a large excess of organic reagent in a sealed tube at 130°C for 4 h, concg. in vacuo; identified by high-pressure chromy. and NMR spectra;
参考文献
Journal of Organometallic Chemistry, , vol. 264, # 1-2 p. 193 - 206
反应条件
in neat (no solvent) Irradiation (UV/VIS); Ge deriv. and a large excess of organic reagent irradiating in a quartztube for 4 h then concg. in vacuo; identified by high-pressure chromy. and NMR spectra;
参考文献
Journal of Organometallic Chemistry, , vol. 264, # 1-2 p. 193 - 206
反应条件
in neat (no solvent) Irradiation (UV/VIS); Ge deriv. and a large excess of organic reagent irradiating in a quartztube for 4 h then concg. in vacuo; identified by high-pressure chromy. and NMR spectra;
参考文献
Journal of Organometallic Chemistry, , vol. 264, # 1-2 p. 193 - 206
反应条件
1: With bromine in tetrachloromethane T=0°C; 3 h; 2: With N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 12 h; Heating;
参考文献
Hingston, Timothy J.; Sambrook, Mark R.; Porfyrakis, Kyriakos; Briggs, G. Andrew D.
Tetrahedron Letters, 2006 , vol. 47, # 42 p. 7413 - 7415
反应条件
in toluene T=110°C; 15 h;
参考文献
Journal of the American Chemical Society, , vol. 117, # 46 p. 11592 - 11593
反应条件
T=370°C; 0.00194444 h;
参考文献
Maier, G.; Reisenauer, H. P.; Schoettler, K.; Wessolek-Kraus, U.
Journal of Organometallic Chemistry, 1989 , vol. 366, p. 25 - 38
参考文献
Ciba Geigy Corporation
Patent: US4139560 A1, 1979 ;
反应条件
Tl(NO3)3*3H2O in methanol; dichloromethane 1 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 997 - 1000
