2,3-二甲基-1,3-丁二烯合成路线 （共 777 条）
反应条件
in benzene
Irradiation;
参考文献
Ishikawa,M. et al.
Journal of Organometallic Chemistry, 1976 , vol. 118, p. 139 - 153
反应条件
in benzene
Irradiation;
参考文献
Ishikawa,M. et al.
Journal of Organometallic Chemistry, 1976 , vol. 118, p. 139 - 153
反应条件
lithium tert-butylate
1. 0 deg C, THF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bates, Robert B.; Gordon, Bernard; Highsmith, Thomas K.; White, James J.
Journal of Organic Chemistry, 1984 , vol. 49, # 16 p. 2981 - 2987
反应条件
in cyclohexane
Irradiation (UV/VIS); 20 molar equivalents of diene, 110-W low pressure Hg arc lamp (254nm, spiral type), 293K, 30min, under Ar;; detn. by GLC and GC-MS;;
参考文献
Mochida, Kunio; Kanno, Naoko; Kato, Ryuji; Kotani, Masahiro; Yamauchi, Seigo; et al.
Journal of Organometallic Chemistry, 1991 , vol. 415, # 2 p. 191 - 201
反应条件
in cyclohexane
Irradiation (UV/VIS); soln. of germane and 20-fold excess of butadiene in dry cyclohexane (quartz tube) degassed, Ar inserted, irradiation (110 W low-pressure Hg arc lamp, room temp., 3 h);
参考文献
Mochida, Kunio; Tokura, Satoshi
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 6 p. 1642 - 1647
反应条件
phenyllithium in diethyl ether
T=-78 - 20°C;
参考文献
Wiberg, Nils; Wagner, Susanne; Vasisht, Sham-Kumar; Polborn, Kurt
Canadian Journal of Chemistry, 2000 , vol. 78, # 11 p. 1412 - 1420
反应条件
n-butyllithium in diethyl ether; hexane
Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Wiberg, Nils; Preiner, Gerhard; Schieda, Oswald; Fischer, Gerd
Chemische Berichte, 1981 , vol. 114, # 11 p. 3505 - 3517
反应条件
in diethyl ether
T=80°C; 72 h;
参考文献
Wiberg, Nils; Preiner, G.; Wagner, G.; Koepf, H.; Fischer, G.
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1987 , vol. 42, # 9 p. 1055 - 1061
反应条件
in diethyl ether
T=80°C; 72 h;
参考文献
Wiberg, Nils; Preiner, G.; Wagner, G.; Koepf, H.; Fischer, G.
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1987 , vol. 42, # 9 p. 1055 - 1061
反应条件
in diethyl ether
Ambient temperature; Yield given;
参考文献
Wiberg, Nils; Koepf, Hubert
Journal of Organometallic Chemistry, 1986 , vol. 315, p. 9 - 18
