2,3-二甲基-1,3-丁二烯合成路线 (共 777 条)
反应条件
chlorine in dichloromethane
T=-78°C; 2 h; Further byproducts given;
参考文献
Said,E.Z.; Tipping,A.E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1972 , p. 1986 - 1991
反应条件
hydroquinone in acetonitrile
T=145°C;
参考文献
Bonjouklian,R.; Ruden,R.A.
Journal of Organic Chemistry, 1977 , vol. 42, # 25 p. 4095 - 4103
反应条件
α-octadecene in hexane
3.5 h; Ambient temperatureIrradiation;
参考文献
Ishikawa, Mitsuo; Nakagawa, Ken-Ichi; Enokida, Ryuichi; Kumada, Makoto
Journal of Organometallic Chemistry, 1980 , vol. 201, # 1 p. 151 - 163
反应条件
tetra-n-butylammonium perchlorate in ethylene glycol dimethyl ether
electrolysis, electrolytic reduction;
参考文献
Kunai, Atsutaka; Ueda, Takafumi; Toyoda, Eiji; Ishikawa, Mitsuo
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 1 p. 287 - 289
反应条件
1: ethanol
2: Ac2O; H3PO4 / 125 °C
View Scheme
参考文献
Fabrizio, Eve F.; Payne, Andrew; Westlund, Neil E.; Bard, Allen J.; Magnus, Philip P.
Journal of Physical Chemistry A, 2002 , vol. 106, # 10 p. 1961 - 1968
参考文献
Bouillon, Jean-Philippe; Musyanovich, Rostyslav; Portella, Charles; Shermolovich, Yuriy
European Journal of Organic Chemistry, 2001 , # 19 p. 3625 - 3629
参考文献
Santini,C.C.; Fischer,J.; Mathey,F.
Journal of the American Chemical Society, 1980 , vol. 102, p. 5809
参考文献
Apitz, Joerg; Grobe, Joseph; Le Van, Duc
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1988 , vol. 43, # 3 p. 257 - 260
反应条件
1: BuLi / tetrahydrofuran; hexane
2: sulfur / benzene / Heating
View Scheme
参考文献
Mathey,F.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1969 , vol. 269, p. 1066 - 1068
反应条件
in chloroform-d1
29 h; Heating; Further byproducts given;
参考文献
Ishii, Akihiko; Oshida, Hideaki; Nakayama, Juzo
Tetrahedron Letters, 2001 , vol. 42, # 17 p. 3117 - 3119