4-丁氧基-3-甲氧基苯甲醛合成路线 （共 7 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=85°C; 24 h; Inert atmosphere;
参考文献
Zhang, Qiang; Peng, Hanqing; Zhang, Guishan; Lu, Qiongqiong; Chang, Jian; Dong, Yeye; Shi, Xianying; Wei, Junfa
Journal of the American Chemical Society, 2014 , vol. 136, # 13 p. 5057 - 5064
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 1 h; Heating;
参考文献
Lee, Eun; Lee, Chulbom; Tae, Jin Sung; Whang, Ho Sung; Li, Kap Sok
Tetrahedron Letters, 1993 , vol. 34, # 14 p. 2343 - 2346
反应条件
1: potassium carbonate; potassium iodide / ethanol / 15 h / |Reflux 2: trichlorophosphate / 19 h / 100 - 115 °C / |Cooling with ice View Scheme
参考文献
Huang, Wei-Bin; Du, Cai-Yan; Jiang, Jian-An; Ji, Ya-Fei
Research on Chemical Intermediates, 2013 , vol. 39, # 6 p. 2849 - 2856
反应条件
trichlorophosphate T=100 - 115°C; Vilsmeier-Haack Formylation; 19 h; Cooling with ice; Overall yield = 83.1 percent; Overall yield = 6.8 g;
参考文献
Huang, Wei-Bin; Du, Cai-Yan; Jiang, Jian-An; Ji, Ya-Fei
Research on Chemical Intermediates, 2013 , vol. 39, # 6 p. 2849 - 2856
参考文献
Kubiczek; Pohl; Smahel
Monatshefte fuer Chemie, 1947 , vol. 77, p. 54
Full Text Show Details
Boeeseken; Greup
Recueil des Travaux Chimiques des Pays-Bas, 1939 , vol. 58, p. 528,532, 535
反应条件
AlCl3, aluminium chloride in dichloromethane T=20°C; 5 h;
参考文献
Huang, Wei-Bin; Du, Cai-Yan; Jiang, Jian-An; Ji, Ya-Fei
Research on Chemical Intermediates, 2013 , vol. 39, # 6 p. 2849 - 2856
反应条件
potassium permanganate
参考文献
Pashkovskii; Shchukina; Gribovskii; Lakhvich
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 5 p. 657 - 670
