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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
51310-29-3
合成路线
（共 6 条）
591-50-4
碘苯
+
201230-82-2
+
5467-74-3
4-溴苯硼酸
→
反应条件
51310-29-3
反应条件
potassium carbonate; bis-triphenylphosphine-palladium(II) chloride in various solvent(s) T=80°C; 5 h;
参考文献
Ishiyama; Kizaki; Miyaura; Suzuki
Tetrahedron Letters, 1993 , vol. 34, # 47 p. 7595 - 7598
67-56-1
甲醇
+
51310-30-6
→
反应条件
51310-29-3
反应条件
sulfuric acid Heating;
参考文献
Pitts, Jonathan D.; Howell, Amy R.; Taboada, Rosa; Banerjee, Ipsita; Wang, Jun; Goodman, Steven L.; Campagnola, Paul J.
Photochemistry and Photobiology, 2002 , vol. 76, # 2 p. 135 - 144
106-38-7
对溴甲苯
→
反应条件
51310-29-3
反应条件
1.1: Mg / diethyl ether / Heating 1.2: 62 percent / diethyl ether / 0.5 h / Heating 2.1: 67 percent / KMnO4 / H2O / 5 h / Heating 3.1: 78 percent / chromic acid; conc. H2SO4 / H2O; acetic acid / Heating 4.1: 81 percent / conc. H2SO4 / Heating View Scheme
参考文献
Pitts, Jonathan D.; Howell, Amy R.; Taboada, Rosa; Banerjee, Ipsita; Wang, Jun; Goodman, Steven L.; Campagnola, Paul J.
Photochemistry and Photobiology, 2002 , vol. 76, # 2 p. 135 - 144
29334-17-6
→
反应条件
51310-29-3
反应条件
1: 67 percent / KMnO4 / H2O / 5 h / Heating 2: 78 percent / chromic acid; conc. H2SO4 / H2O; acetic acid / Heating 3: 81 percent / conc. H2SO4 / Heating View Scheme
参考文献
Pitts, Jonathan D.; Howell, Amy R.; Taboada, Rosa; Banerjee, Ipsita; Wang, Jun; Goodman, Steven L.; Campagnola, Paul J.
Photochemistry and Photobiology, 2002 , vol. 76, # 2 p. 135 - 144
76693-57-7
4-溴-4-甲基苯甲酮
→
反应条件
51310-29-3
反应条件
1: 78 percent / chromic acid; conc. H2SO4 / H2O; acetic acid / Heating 2: 81 percent / conc. H2SO4 / Heating View Scheme
参考文献
Pitts, Jonathan D.; Howell, Amy R.; Taboada, Rosa; Banerjee, Ipsita; Wang, Jun; Goodman, Steven L.; Campagnola, Paul J.
Photochemistry and Photobiology, 2002 , vol. 76, # 2 p. 135 - 144
1122-91-4
4-溴苯甲醛
→
反应条件
51310-29-3
反应条件
1.1: Mg / diethyl ether / Heating 1.2: 62 percent / diethyl ether / 0.5 h / Heating 2.1: 67 percent / KMnO4 / H2O / 5 h / Heating 3.1: 78 percent / chromic acid; conc. H2SO4 / H2O; acetic acid / Heating 4.1: 81 percent / conc. H2SO4 / Heating View Scheme
参考文献
Pitts, Jonathan D.; Howell, Amy R.; Taboada, Rosa; Banerjee, Ipsita; Wang, Jun; Goodman, Steven L.; Campagnola, Paul J.
Photochemistry and Photobiology, 2002 , vol. 76, # 2 p. 135 - 144
