4-四氢吡喃基氧基-丁烷-1-醇合成路线 (共 25 条)
反应条件
1: 83 percent / PPh3; imidazole; iodine / benzene; diethyl ether / 1 h / 20 °C
2: 2.6 g / benzene / 36 h / 80 °C
View Scheme
参考文献
Curran, Dennis P.; Furukawa, Takashi
Organic Letters, 2002 , vol. 4, # 13 p. 2233 - 2235
反应条件
pyridine in chloroform
T=0°C; 4 h;
参考文献
Breen, Anthony P.; Murphy, John A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 23 p. 2979 - 2990
反应条件
1: pyridinium chlorochromate / CH2Cl2
2: benzene
3: LiAl(OC2H5)2H2 / diethyl ether
4: pyridinium chlorochromate / CH2Cl2
View Scheme
参考文献
Sharma, G. V. M.; Shekharam, T.; Upender, V.
Tetrahedron, 1990 , vol. 46, # 16 p. 5665 - 5672
反应条件
1: 85 percent / PCC / CH2Cl2
2: 70 percent / tetrahydrofuran / 1 h / Heating
View Scheme
参考文献
Inoue, Hirohumi; Murata, Shizuaki; Suzuki, Toshiyasu
Liebigs Annalen der Chemie, 1994 , # 9 p. 901 - 910
反应条件
1H-imidazole; iodine; triphenylphosphine in tetrahydrofuran
T=-30 - 20°C; Inert atmosphere;
参考文献
Liblikas, Ilme; Mozuraitis, Raimondas; Santangelo, Ellen M.; Noreika, Remigijus; Borg-Karlson, Anna-Karin
Chemistry and Biodiversity, 2009 , vol. 6, # 9 p. 1388 - 1403