反应条件
1: 1.) SOCl2 2.) tetrabutylammonium azide / 1.) SOCl2, benzene, 48 h, RT 2.) tetrabutylammonium azide, acetonitrile, 1 h, RT
2: 53 percent / xylene / Heating
View Scheme
参考文献
Takeuchi, Hisato; Eguchi, Shoji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2149 - 2154