1: 1,3,5-tribromo benzene With magnesium in tetrahydrofuran
T=20°C; 2 h;
2: benzoyl chloride With bis[2-(N,N-dimethylamino)ethyl] ether in tetrahydrofuran
T=0°C; 4 h;
3: With hydrogenchloride; water
pH=5;
参考文献
TRANSITIONS OPTICAL, INC.
Patent: WO2012/82506 A1, 2012 ;
Location in patent: Page/Page column 49 ;
Waters
Journal of the Chemical Society, 1929 , p. 2108
Full Text Show Details
Montagne
Recueil des Travaux Chimiques des Pays-Bas, 1922 , vol. 41, p. 718
Recueil des Travaux Chimiques des Pays-Bas, 1923 , vol. 42, p. 506
