N-苄基-N-(2-甲氧基乙基)胺合成路线 （共 7 条）
反应条件
1-(3-amino-2,4-dihydroxy-phenyl)-ethanone in methanol
T=20°C; 4 h; Inert atmosphereElectrochemical reaction; chemoselective reaction;
参考文献
Largeron, Martine; Fleury
Organic Letters, 2009 , vol. 11, # 4 p. 883 - 886
反应条件
1: With [RuN(saldach)(CH3OH)](+)[ClO4](-); phenyl silane in toluene
12 h; Reflux;
2: With hydrogenchloride in diethyl ether; water; toluene
参考文献
Abbina, Srinivas; Bian, Shi; Oian, Casey; Du, Guodong
ACS Catalysis, 2013 , vol. 3, # 4 p. 678 - 684
反应条件
1: With hydrogenchloride in diethyl ether
T=23°C; 1 h; Inert atmosphere;
2: With sodium hydrogencarbonate in methanol; water
T=23°C; 2 h; Inert atmosphere;
参考文献
Cheng, Chen; Brookhart, Maurice
Journal of the American Chemical Society, 2012 , vol. 134, # 28 p. 11304 - 11307
反应条件
titanium tetrachloride; magnesium; mercury dichloride in tetrahydrofuran
T=0°C; 12 h; Yields of byproduct given;
参考文献
Mangeney, P.; Tejero, T.; Alexakis, A.; Grosjean, F.; Normant, J.
Synthesis, 1988 , # 3 p. 255 - 257
反应条件
1: 97 percent / molecular sieves 4 Angstroem / CH2Cl2 / 1 h / Ambient temperature
2: HgCl2, Mg, TiCl4 / tetrahydrofuran / 12 h / 0 °C
View Scheme
参考文献
Mangeney, P.; Tejero, T.; Alexakis, A.; Grosjean, F.; Normant, J.
Synthesis, 1988 , # 3 p. 255 - 257
反应条件
hydrogenchloride; sodium cyanoborohydride in water; acetonitrile
72 h; Ambient temperature;
参考文献
McGill
Synthesis, 1993 , # 11 p. 1089 - 1091
反应条件
1.1: [Ir(μ-Cl)(cyclooctene)2]2; diethylesilane / 5 h / 23 °C / Inert atmosphere
2.1: hydrogenchloride / diethyl ether / 1 h / 23 °C / Inert atmosphere
2.2: 2 h / 23 °C / Inert atmosphere
View Scheme
参考文献
Cheng, Chen; Brookhart, Maurice
Journal of the American Chemical Society, 2012 , vol. 134, # 28 p. 11304 - 11307
