2,7-二甲氧基萘-1-甲醛合成路线 （共 12 条）
反应条件
water; silver(l) oxide
参考文献
Buu-Hoi; Lavit
Journal of the Chemical Society, 1956 , p. 1743,1748
反应条件
1: 87 percent / AlCl3 / CH2Cl2 / 3 h / Ambient temperature
2: benzene / Heating
3: benzene / 1.) 15 h, room temp., 2.) 1 h, reflux
View Scheme
参考文献
Royer; Buisson
European Journal of Medicinal Chemistry, 1980 , vol. 15, # 3 p. 275 - 278
反应条件
hydrazine hydrate; diethylene glycol
anschliessendes Erhitzen mit KOH;
参考文献
Cannon, Jack R.; Feutrill, Geoffrey I.; Wong, Laurence C. H.
Australian Journal of Chemistry, 1983 , vol. 36, # 12 p. 2575 - 2580
反应条件
1: 1.) diethylene glycol, 99 percent hydrazine hydrate, 2.) KOH / 1.) 100 deg C, 5 min, 2.) 170-180 deg C, 1 h
2: 90 mg / 1.) ethanethiol, NaH, 3.) pyridine / 1.) DMF, 2.) 140 deg C, 3 h, 3.) a.) 100 deg C, 10 min, b.) RT, overnight
View Scheme
参考文献
Cannon, Jack R.; Feutrill, Geoffrey I.; Wong, Laurence C. H.
Australian Journal of Chemistry, 1983 , vol. 36, # 12 p. 2575 - 2580
反应条件
hydrogenchloride; titanium tetrachloride
1.) a) CH2Cl2, 0 deg C, 1 h, b) RT, 4 h; Yield given. Multistep reaction;
参考文献
Langlois, Michel; Bremont, Beatrice; Shen, Shuren; Poncet, Annie; Andrieux, Jean; et al.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 12 p. 2050 - 2060
反应条件
trichlorophosphate in 1,2-dichloro-ethane
T=100°C; 11 h;
参考文献
Mizutani, Tadashi; Murakami, Takeshi; Kurahashi, Takuya; Ogoshi, Hisanobu
Journal of Organic Chemistry, 1996 , vol. 61, # 2 p. 539 - 548
反应条件
trichlorophosphate
Vilsmeier-Haack reaction; 0.05 h; Microwave irradiation;
参考文献
Ghosh, Kumaresh; Adhikari, Suman
Journal of the Indian Chemical Society, 2008 , vol. 85, # 9 p. 959 - 961
反应条件
manganese triacetate in acetic acid
0.0166667 h; Heating;
参考文献
Nishino, Hiroshi; Tsunoda, Katsunori; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 2 p. 545 - 550
参考文献
Adams et al.
Journal of the American Chemical Society, 1942 , vol. 64, p. 1795,1800
参考文献
Adams et al.
Journal of the American Chemical Society, 1942 , vol. 64, p. 1795,1800
