2-(烯丙基硫代)苯并咪唑合成路线 (共 17 条)
反应条件
N-ethyl-N,N-diisopropylamine in acetone
T=20°C; 0.05 h; Sonication;
参考文献
Deligeorgiev, Todor; Kaloyanova, Stefka; Lesev, Nedyalko; Vaquero, Juan J.
Ultrasonics Sonochemistry, 2010 , vol. 17, # 5 p. 783 - 788
反应条件
potassium hydroxide in water
1 h;
参考文献
Kim; Avdin; Gavrilova
Chemistry of Heterocyclic Compounds, 1997 , vol. 33, # 8 p. 986 - 988
反应条件
sodium hydroxide; Amberlite IRA-400 chloride form in water; acetone
参考文献
Dalal; Pawar; Mahulikar
Organic Preparations and Procedures International, 2005 , vol. 37, # 6 p. 539 - 546
反应条件
tris-(dibenzylideneacetone)dipalladium(0); 1,4-di(diphenylphosphino)-butane in tetrahydrofuran
T=5°C; 24 h;
参考文献
Goux, Catherine; Sigismondi, Silvana; Sinou, Denis
Journal of Chemical Research, Miniprint, 1997 , # 11 p. 2308 - 2317
反应条件
potassium hydroxide; Diquat in dichloromethane; water
Alkylation; 1.5 h;
参考文献
Jayachandran, J. Paul; Wang, Maw-Ling
Synthetic Communications, 1999 , vol. 29, # 23 p. 4087 - 4099
反应条件
1: reconstructed hydrotalcite / ethanol; water / 0.42 h / 70 °C / 2250.23 - 3000.3 Torr / |Microwave irradiation; |Cooling
2: reconstructed hydrotalcite / ethanol / 0.58 h / 70 °C / |Microwave irradiation; |Cooling
View Scheme
参考文献
Cruz-Gonzalez, Deysi Y.; Gonzalez-Olvera, Rodrigo; Angeles-Beltran, Deyanira; Negron-Silva, Guillermo E.; Santillan, Rosa
Synthesis (Germany), 2013 , vol. 45, # 23 p. 3281 - 3287
反应条件
1: reconstructed hydrotalcite / ethanol; water / 0.42 h / 70 °C / 2250.23 - 3000.3 Torr / |Microwave irradiation; |Cooling
2: reconstructed hydrotalcite / ethanol / 3 h / 70 °C / |Microwave irradiation; |Cooling
View Scheme
参考文献
Cruz-Gonzalez, Deysi Y.; Gonzalez-Olvera, Rodrigo; Angeles-Beltran, Deyanira; Negron-Silva, Guillermo E.; Santillan, Rosa
Synthesis (Germany), 2013 , vol. 45, # 23 p. 3281 - 3287