反应条件
1: NBS / acetone / 6 h / Irradiation
2: dimethylformamide
3: 1.) NaOEt, 2.) I2 / 1.) EtOH, 30-50 deg C, 30 min; reflux, 1 h, 2.) heptane, irradiation
4: 10 percent / K2OsO4*2H2O, quinine 4-chlorobenzoate, K3<Fe(CN)6>, K2CO3 / H2O; 2-methyl-propan-2-ol / 48 h / Ambient temperature
View Scheme
参考文献
Terfort, Andreas; Brunner, Henri
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 12 p. 1467 - 1479
