in tetrahydrofuran
under inert atm. soln. NaBAr4 in THF was added dropwise at room temp. toBi(III) carboxylate in the same solvent and refluxed for 16 h; solvent was removed in vacuo, residue was extd. into hexane, filtered and subjected to column chromy. on silica (pentane-CH2Cl2 90:10);
参考文献
Stavila, Vitalie; Thurston, John H.; Prieto-Centurion, Dario; Whitmire, Kenton H.
Organometallics, 2007 , vol. 26, # 27 p. 6864 - 6866
