5,7-双(三氟甲基)[1,8]萘啶-2-醇合成路线 （共 4 条）
反应条件
sulfuric acid; sodium nitrite in acetic acid 24 h; Reflux;
参考文献
Harada, Naomi; Abe, Yuichiro; Karasawa, Satoru; Koga, Noboru
Organic Letters, 2012 , vol. 14, # 24 p. 6282 - 6285
反应条件
1: 95 percent / 85percent phosphoric acid / 12 h / 60 °C / sealed tube 2: 1) conc.H2SO4, sodium nitrite; 2) water / 1) RT, 12 h; 2) boiling steam bath, 30 min View Scheme
参考文献
Harada, Naomi; Abe, Yuichiro; Karasawa, Satoru; Koga, Noboru
Organic Letters, 2012 , vol. 14, # 24 p. 6282 - 6285
反应条件
1: 95 percent / 85percent phosphoric acid / 12 h / 60 °C / sealed tube 2: 1) conc.H2SO4, sodium nitrite; 2) water / 1) RT, 12 h; 2) boiling steam bath, 30 min View Scheme
参考文献
Harada, Naomi; Abe, Yuichiro; Karasawa, Satoru; Koga, Noboru
Organic Letters, 2012 , vol. 14, # 24 p. 6282 - 6285
反应条件
trichlorophosphate in N,N-dimethyl-formamide T=100°C; 1.5 h; Cooling with ice;
参考文献
Organic Letters, , vol. 14, # 24 p. 6282 - 6285
