tert-butylhypochlorite; triethylamine trihydrofluoride in hexane
Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Shellhamer, Dale F.; Horney, Mark J.; Pettus, Benjamin J.; Pettus, Tobiah L.; Stringer, Joy Merry; Heasley, Victor L.; Syvret, Robert G.; Dobrolsky Jr., John M.
Journal of Organic Chemistry, 1999 , vol. 64, # 4 p. 1094 - 1098
N,N-dichloro-methylamine; boron trifluoride diethyl etherate in dichloromethane
Ambient temperaturefurther chlorinating agents (for example: (CH3)2NCl ); Yields of byproduct given;
参考文献
Heasley, Gene E.; Janes, J. Mark; Stark, Stephen R.; Robinson, Brian L.; Heasley, Victor L.; Shellhamer, Dale F.
Tetrahedron Letters, 1985 , vol. 26, # 15 p. 1811 - 1814
boron trifluoride diethyl etherate in dichloromethane
T=25°C; 0.0833333 h; var. alkenes, var. hypohalites; other solvent: CCl4, other temp.: -78 degC; var. ratios of hypohalite; Product distribution;
参考文献
Heasley, Victor L.; Gipe, Robert K.; Martin, Jody L.; Wiese, Harry C.; Oakes, Melanie L.; Shellhamer, Dale F.
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3195 - 3199
Heasley, Gene E.; Janes, J. Mark; Stark, Stephen R.; Robinson, Brian L.; Heasley, Victor L.; Shellhamer, Dale F.
Tetrahedron Letters, 1985 , vol. 26, # 15 p. 1811 - 1814