2,3-二氯-1,4-苯醌合成路线 （共 21 条）
反应条件
hydrogenchloride in chloroform
24 h; Ambient temperature;
参考文献
Claramunt, R. M.; Escolastico, C.; Maria, M. D. Santa; Lopez, V.
Anales de Quimica, 1994 , vol. 90, # 5-6 p. 368 - 371
反应条件
Erwaermen des in Essigsaeure geloesten Reaktionsprodukts mit K2Cr2O7 und wss. H2SO4;
参考文献
Gen. Aniline Works
Patent: US1891168 , 1929 ;
Full Text Show Details
I.G. Farbenind.
Patent: GB324661 , 1928 ;
反应条件
1: With sulfuryl dichloride in diethyl ether; chloroform
T=0°C; 0.5 h; Inert atmosphere;
2: With silver(l) oxide in diethyl ether
1 h;
参考文献
SLOAN-KETTERING INSTITUTE FOR CANCER RESEARCH; DJABALLAH, Hakim; ANTCZAK, Christophe
Patent: WO2010/129049 A1, 2010 ;
Location in patent: Page/Page column 111; 113 ;
WO 2010/129049 A1
反应条件
silver(l) oxide in diethyl ether
T=25°C; 0.5 h;
参考文献
Pochorovski, Igor; Boudon, Corinne; Gisselbrecht, Jean-Paul; Ebert, Marc-Olivier; Schweizer, W. Bernd; Diederich, Francois
Angewandte Chemie - International Edition, 2012 , vol. 51, # 1 p. 262 - 266
参考文献
Eistert,B. et al.
Chemische Berichte, 1975 , vol. 108, p. 693 - 699
反应条件
1: diethyl ether; hydrogen chloride
2: manganese dioxide; sulfuric acid
View Scheme
参考文献
Conant; Fieser
Journal of the American Chemical Society, 1923 , vol. 45, p. 2205
Journal of the American Chemical Society, 1924 , vol. 46, p. 1877 Anm. 43
反应条件
1: granulated zinc; sulfur dioxide; diluted acetic acid / man oxydiert das Reaktionsprodukt mit Kaliumdichromat, Eis und Schwefelsaeure
2: diethyl ether; hydrogen chloride
3: manganese dioxide; sulfuric acid
View Scheme
参考文献
Conant; Fieser
Journal of the American Chemical Society, 1923 , vol. 45, p. 2205
Journal of the American Chemical Society, 1924 , vol. 46, p. 1877 Anm. 43
反应条件
boron trifluoride; silver(l) oxide
Multistep reaction;
参考文献
Park, Aeri; Schmitz, Francis J.
Tetrahedron Letters, 1993 , vol. 34, # 25 p. 3983 - 3984
反应条件
Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Yu, Duyi; Mattern, Daniell Lewis
Synthetic Communications, 1999 , vol. 29, # 5 p. 821 - 825
反应条件
in ethanol; water
T=25°C; 16 h; Rate constantMechanismProduct distribution;
参考文献
Atkinson, Romily C.; Mare, Peter B. D. de la; Larsen, David S.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 271 - 280
