六-O-乙酰基-呋喃葡烯糖-5-半乳糖甘合成路线 (共 8 条)
反应条件
β-cyclodextrin; zinc in water T=20°C; 1.5 h; Sonication;
参考文献
Zhao, Jinzhong; Shao, Huawu; Wu, Xin; Shi, Shaojing
Chinese Journal of Chemistry, 2011 , vol. 29, # 7 p. 1434 - 1440
反应条件
1: With iodine in dichloromethane 0.166667 h; Reflux; 2: With bis(cyclopentadienyl)titanium dichloride; manganese in tetrahydrofuran T=20°C; 1 h; Inert atmosphere;
参考文献
Giordano, Maddalena; Iadonisi, Alfonso
European Journal of Organic Chemistry, 2013 , # 1 p. 125 - 131
反应条件
cyanocobalamin; ammonium chloride; zinc in methanol 0.0833333 h;
参考文献
Ruhela, Dipali; Vishwakarma, Ram A.
Journal of Organic Chemistry, 2003 , vol. 68, # 11 p. 4446 - 4456
反应条件
tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide 0.333333 h; Ambient temperature;
参考文献
De Pouilly, Pierre; Chenede, Alain; Mallet, Jean-Maurice; Sinay, Pierre
Tetrahedron Letters, 1992 , vol. 33, # 52 p. 8065 - 8068
反应条件
sodium acetate; copper(II) sulfate; acetic acid; zinc 1.5 h; Yield given;
参考文献
Journal of Carbohydrate Chemistry, , vol. 15, # 8 p. 955 - 964
反应条件
1: copper(II) bis(trifluoromethanesulfonate) / 12 h / 20 °C / Neat (no solvent) 2: hydrogen bromide / acetic acid / 5 °C 3: sodium acetate; copper(II) sulfate; zinc / acetic acid / 5 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 21, # 4 p. 1265 - 1269
反应条件
sodium carbonate in methanol 2 h; Ambient temperature;
参考文献
Upreti, Mani; Vishwakarma, Ram A.
Tetrahedron Letters, 1999 , vol. 40, # 13 p. 2619 - 2622
反应条件
[C2mim][CH3SO4] in acetonitrile T=25°C; pH=5; 26 h; aq. acetate bufferEnzymatic reaction; regioselective reaction;
参考文献
Green Chemistry, , vol. 12, # 8 p. 1365 - 1369