2-(6,7-二甲氧基-1,2,3,4-四氢-异喹啉-1-基)乙醇合成路线 （共 4 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=25°C; 4 h;
参考文献
Tietze, Lutz F.; Rackelmann, Nils; Mueller
Chemistry - A European Journal, 2004 , vol. 10, # 11 p. 2722 - 2731
反应条件
1: 93 percent / H2 / Pd/C / acetic acid; ethanol / 1.33 h / 3075.25 Torr
2: 92 percent / LiAlH4 / tetrahydrofuran / 4 h / 25 °C
View Scheme
参考文献
Tietze, Lutz F.; Rackelmann, Nils; Mueller
Chemistry - A European Journal, 2004 , vol. 10, # 11 p. 2722 - 2731
反应条件
1: 83 percent / P4O10 / toluene / 1.17 h / 110 °C
2: 93 percent / H2 / Pd/C / acetic acid; ethanol / 1.33 h / 3075.25 Torr
3: 92 percent / LiAlH4 / tetrahydrofuran / 4 h / 25 °C
View Scheme
参考文献
Tietze, Lutz F.; Rackelmann, Nils; Mueller
Chemistry - A European Journal, 2004 , vol. 10, # 11 p. 2722 - 2731
反应条件
1: 91 percent / aq. K2CO3 / diethyl ether / 1.5 h / 0 °C
2: 83 percent / P4O10 / toluene / 1.17 h / 110 °C
3: 93 percent / H2 / Pd/C / acetic acid; ethanol / 1.33 h / 3075.25 Torr
4: 92 percent / LiAlH4 / tetrahydrofuran / 4 h / 25 °C
View Scheme
参考文献
Tietze, Lutz F.; Rackelmann, Nils; Mueller
Chemistry - A European Journal, 2004 , vol. 10, # 11 p. 2722 - 2731
