[双(甲硫基)亚甲基]丙烷二腈合成路线 （共 52 条）
反应条件
triethylamine 0.05 h; Heating;
参考文献
Erdmann, Barbara; Knoll, A.; Liebscher, J.
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 6 p. 1015 - 1021
反应条件
1: 1.) 50percent NaH / 1.) benzene, N,N-dimethylacetamide, room temperature; 2.) methanol, reflux 2: 66 percent / POCl3, N,N-dimethylaniline / Heating View Scheme
参考文献
Kohra, Shinya; Tominaga, Yoshinori; Hosomi, Akira
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 959 - 968
反应条件
potassium carbonate in N,N-dimethyl-formamide 5 h; Reflux;
参考文献
Vartale, Sambhaji P.; Halikar, Nilesh K.; Sirsat, Shivraj B.; Pawar, Yogesh D.
Journal of Heterocyclic Chemistry, 2013 , vol. 50, # 2 p. 351 - 354
反应条件
in water
Reflux; regioselective reaction;
参考文献
Chanu, Langpoklakpam Gellina; Singh, Okram Mukherjee; Jang, Sang Hun; Lee, Sang-Gyeong
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 4 p. 859 - 862
反应条件
in methanol
15 h; Heating;
参考文献
Mukaiyama, Harunobu; Nishimura, Toshihiro; Shiohara, Hiroaki; Kobayashi, Satoko; Komatsu, Yoshimitsu; Kikuchi, Shinji; Tsuji, Eiichi; Kamada, Noboru; Ohnota, Hideki; Kusama, Hiroshi
Chemical and Pharmaceutical Bulletin, 2007 , vol. 55, # 6 p. 881 - 889
反应条件
in methanol
15 h; Heating;
参考文献
Mukaiyama, Harunobu; Nishimura, Toshihiro; Shiohara, Hiroaki; Kobayashi, Satoko; Komatsu, Yoshimitsu; Kikuchi, Shinji; Tsuji, Eiichi; Kamada, Noboru; Ohnota, Hideki; Kusama, Hiroshi
Chemical and Pharmaceutical Bulletin, 2007 , vol. 55, # 6 p. 881 - 889
反应条件
1: ethanol / Heating
2: m-chloroperbenzoic acid / CH2Cl2 / 20 °C
3: H2O2; NaOH / H2O / 0 - 40 °C
View Scheme
参考文献
Katiyar, Sanjay Babu; Kumar, Arun; Chauhan, Prem M. S.
Synthetic Communications, 2006 , vol. 36, # 20 p. 2963 - 2973
反应条件
potassium fluoride on basic alumina in acetonitrile
1 h; Heating;
参考文献
Yu, Shen-Yi; Cai, Ya-Xian
Synthetic Communications, 2003 , vol. 33, # 22 p. 3989 - 3995
参考文献
Middleton et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 2822,2826
反应条件
in ethanol
24 h; Heating;
参考文献
El-Shafei, Ahmed Kamal; Soliman, Ahmed Mohamed; Sultan, Adel Abdel-Rahim; El-Saghier, Ahmed Mohamed Mohamed
Gazzetta Chimica Italiana, 1995 , vol. 125, # 3 p. 115 - 118
