6-(羟基甲基)-3-[(4-甲氧基苯基)亚甲基氨基]四氢吡喃-2,4,5-三醇合成路线 （共 5 条）
反应条件
1: pyridine / 48 h / 20 °C 2: 90 percent / aq. HCl / acetone / 0 °C / pH 5 View Scheme
参考文献
Tao, Chuan-Zhou; Zhang, Zhong-Tang; Wu, Jian-Wei; Li, Rong-Hua; Cao, Zhi-Ling
Chinese Chemical Letters, 2014 , vol. 25, # 4 p. 532 - 534
反应条件
1: pyridine / 48 h / 20 °C 2: 90 percent / aq. HCl / acetone / 0 °C / pH 5 View Scheme
参考文献
Tao, Chuan-Zhou; Zhang, Zhong-Tang; Wu, Jian-Wei; Li, Rong-Hua; Cao, Zhi-Ling
Chinese Chemical Letters, 2014 , vol. 25, # 4 p. 532 - 534
反应条件
1: 81 percent / pyridine / 6 h / 0 - 40 °C 2: 90 percent / HCl/MeOH / acetone / 1 h / 25 °C 3: 1.) Et3N / 1.) pyridine, 75 min, 2.) 90-95 deg C, 10 min View Scheme
参考文献
Tetrahedron, , vol. 53, # 12 p. 4159 - 4178
反应条件
1: 72 percent / pyridine / 20 °C 2: 100 percent / HCl / acetone 3: 83 percent / NaHCO3 / CHCl3; H2O / pH 8.0 View Scheme
参考文献
Kyas, Andreas; Feigel, Martin
Helvetica Chimica Acta, 2005 , vol. 88, # 9 p. 2375 - 2396
反应条件
1: 90 percent / pyridine
2: 90 percent / HCl / acetone
3: 90 percent
4: 80 percent / BF3*Et2O
5: 40 percent / DMTST, molecular sieves
6: Zn
7: H2 / Pd
View Scheme
参考文献
Simanek, Eric E.; Huang, Dee-Hua; Pasternack, Laura; Machajewski, Timothy D.; Seitz, Oliver; Millar, David S.; Jane Dyson; Wong, Chi-Huey
Journal of the American Chemical Society, 1998 , vol. 120, # 45 p. 11567 - 11575
