3-氰基-7-(二乙基氨基)香豆素合成路线 （共 15 条）
反应条件
sulfuric acid; water 1) frrom 90 deg C to 95 deg C, 40 min, 2.) reflux, 40 min; Yield given. Multistep reaction;
参考文献
Tkach, I. I.; Reznichenko, A. V.; Luk'yanets, E. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 8 p. 872 - 880
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 8 p. 1043 - 1052
反应条件
sulfuric acid 8 h; Heating;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 28, # 8 p. 872 - 880
Khimiya Geterotsiklicheskikh Soedinenii, , # 8 p. 1043 - 1052
反应条件
amino acid fuctionalized Fe3O4 nanoparticles(Fe3O4-DA-Phe) in neat (no solvent)
T=130°C; Knoevenagel Condensation; 0.1 h; Microwave irradiationGreen chemistry;
参考文献
Girija; Naik, H.S. Bhojya; Kumar, B. Vinay; Sudhamani; Harish
Letters in Organic Chemistry, 2013 , vol. 10, # 7 p. 468 - 477
反应条件
1-propanephosphonic acid cyclic anhydride; triethylamine in acetic acid n-butyl ester; ethyl acetate
T=120°C; Perkin condensation;
参考文献
Augustine, John Kallikat; Bombrun, Agnes; Ramappa, Balakrishna; Boodappa, Chandrakantha
Tetrahedron Letters, 2012 , vol. 53, # 33 p. 4422 - 4425
反应条件
piperidine in ethanol
T=70°C; 0.5 h; Inert atmosphere;
参考文献
Li, Ju-Ying; Zhou, Xin-Qi; Zhou, Yi; Fang, Yuan; Yao, Cheng
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2013 , vol. 102, p. 66 - 70
反应条件
zirconium tetrachloride; 1-n-butyl-3-methylimidazolium tetrafluoroborate
T=25°C; Knoevenagel condensation; 0.583333 h;
参考文献
Valizadeh, Hassan; Mahmoodian, Manzar; Gholipour, Hamid
Journal of Heterocyclic Chemistry, 2011 , vol. 48, # 4 p. 799 - 802
反应条件
hydrogenchloride in ethanol
0.333333 h; Heating;
参考文献
Tkach, I. I.; Reznichenko, A. V.; Luk'yanets, E. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 8 p. 872 - 880
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 8 p. 1043 - 1052
反应条件
piperidine in ethanol
0.5 h; Heating;
参考文献
Czerney, P.; Hartmann, H.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 1 p. 21 - 28
反应条件
1-(2-OPPh2-propyl)-3-methylimidazolium hexafluorophosphate
T=60°C; 0.333333 h;
参考文献
Valizadeh, Hassan; Gholipour, Hamid
Synthetic Communications, 2010 , vol. 40, # 10 p. 1477 - 1485
反应条件
1: 49 percent / acetic acid / 1 h / Heating
2: 84 percent / aq. 15percent HCl / ethanol / 0.33 h / Heating
View Scheme
参考文献
Tkach, I. I.; Reznichenko, A. V.; Luk'yanets, E. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 8 p. 872 - 880
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 8 p. 1043 - 1052
