3-(苯硫基)-1,2-丙烷二醇合成路线 (共 20 条)
反应条件
sulfuric acid
Trennung durch Behandlung mit Aether; higher-melting trimolecular β-phenylsulfanyl-propionaldehyde;
参考文献
Hutchison; Smiles
Chemische Berichte, 1914 , vol. 47, p. 806
反应条件
sodium periodate
1 h; Ambient temperature;
参考文献
Ohta, Hiromichi; Miyamae, Yoshitaka; Tsuchihashi, Gen-ichi
Agricultural and Biological Chemistry, 1989 , vol. 53, # 1 p. 215 - 222
反应条件
1,4-diaza-bicyclo[2.2.2]octane; K2lt;OsO2(OH)4gt;; oxygen in water; tert-butyl alcohol
T=50°C; P=750.075 Torr; pH=10.4; 18 h;
参考文献
Doebler, Christian; Mehltretter, Gerald M.; Sundermeier, Uta; Beller, Matthias
Journal of the American Chemical Society, 2000 , vol. 122, # 42 p. 10289 - 10289
反应条件
zinc(II) chloride
T=30°C; pH=4.0; 0.08 h;
参考文献
Amantini, David; Fringuelli, Francesco; Pizzo, Ferdinando; Tortoioli, Simone; Vaccaro, Luigi
Synlett, 2003 , # 15 p. 2292 - 2296
反应条件
titanium(IV) isopropylate in isopropyl alcohol
Ambient temperature;
参考文献
Ko, Soo Y.; Masamune, Hiroko; Sharpless, K. Barry
Journal of Organic Chemistry, 1987 , vol. 52, # 4 p. 667 - 671
反应条件
potassium thiocyanate in neat (no solvent)
T=120°C; 0.333333 h; Microwave irradiation; regioselective reaction;
参考文献
Vaddula, Buchi Reddy; Varma, Rajender S.; Leazer, John
European Journal of Organic Chemistry, 2012 , # 35 p. 6852 - 6855
参考文献
Yale et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 3716
反应条件
sodium methylate in methanol
120 h; Ambient temperature;
参考文献
Fruchier, Alain; Moragues, Veronique; Petrus, Clement; Petrus, Francoise
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 5-6 p. 173 - 182
反应条件
sodium methylate in methanol
120 h; Ambient temperature;
参考文献
Fruchier, Alain; Moragues, Veronique; Petrus, Clement; Petrus, Francoise
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 5-6 p. 173 - 182
反应条件
potassium hydroxide in methanol
Yield given;
参考文献
Samii, Zakaria K. M. Abd El; Ashmawy, Mohamed I. Al; Mellor, John M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2509 - 2516