3-(苯硫基)-1,2-丙烷二醇合成路线 （共 20 条）
反应条件
potassium hydroxide in methanol
Yield given;
参考文献
Samii, Zakaria K. M. Abd El; Ashmawy, Mohamed I. Al; Mellor, John M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2509 - 2516
反应条件
sodium hydroxide
T=20°C; Substitution;
参考文献
Lee, Jae Wook; Lee, Chi-Wan; Jung, Jin Hang; Oh, Dong Young
Synthetic Communications, 2000 , vol. 30, # 16 p. 2897 - 2902
反应条件
1: K2CO3 / acetone / Heating
2: 1N sulfuric acid / 1 h / Ambient temperature
View Scheme
参考文献
Ohta, Hiromichi; Miyamae, Yoshitaka; Tsuchihashi, Gen-ichi
Agricultural and Biological Chemistry, 1989 , vol. 53, # 1 p. 215 - 222
反应条件
in ethanol
T=0 - 5°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Apparao, Satyam; Schmidt, Richard R.
Synthesis, 1987 , # 10 p. 896 - 899
反应条件
sodium hydroxide
T=170°C;
参考文献
Gierer,J.; Wallin,N.-H.
Acta Chemica Scandinavica (1947-1973), 1965 , vol. 19, p. 1502 - 1503
反应条件
sodium hydroxide
T=170°C;
参考文献
Gierer,J.; Wallin,N.-H.
Acta Chemica Scandinavica (1947-1973), 1965 , vol. 19, p. 1502 - 1503
反应条件
sulfuric acid
1 h; Ambient temperature;
参考文献
Ohta, Hiromichi; Miyamae, Yoshitaka; Tsuchihashi, Gen-ichi
Agricultural and Biological Chemistry, 1989 , vol. 53, # 1 p. 215 - 222
反应条件
potassium hydroxide; acetic anhydride
1.) 130 deg C, 1 h, 2.) MeOH, 25 deg C to 30 deg C, 20 min; Multistep reaction;
参考文献
Kalugin, V. E.; Litvinov, V. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 7 p. 1391 - 1394
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 7 p. 1574 - 1578
反应条件
AD-mix-β in water; tert-butyl alcohol
24 h; Ambient temperaturefurther reagents; Product distribution;
参考文献
Sammakia, Tarek; Hurley, T. Brian; Sammond, Douglas M.; Smith, Randall S.; Sobolov, Susan B.; Oeschger, Thomas R.
Tetrahedron Letters, 1996 , vol. 37, # 26 p. 4427 - 4430
参考文献
Hutchison; Smiles
Chemische Berichte, 1914 , vol. 47, p. 806
