反应条件
1: tetrahydrofuran / 6 h / Ambient temperature
2: 1) BuLi / 1) hexane, THF, 2) THF, -78 deg C
3: 1) LiAlH4, 2) 10percent aq. NaOH / 1) -20 deg C, 2 h, THF, hexane, 2) -10 deg C, 1 h, THF, hexane
View Scheme
参考文献
Takahata, Hiroki; Takahashi, Koichi; Wang, Eng-Chi; Yamazaki, Takao
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 1211 - 1214
