2,2,2-三氯-1-乙氧基乙醇合成路线 （共 41 条）
参考文献
Post
Journal of Organic Chemistry, 1941 , vol. 6, p. 831,833
反应条件
1: With hydrogenchloride; sodium sulfate in water
1 h;
2: With hydrazine in water
T=80°C; 1.5 h;
参考文献
MEMORY PHARMACEUTICALS CORPORATION
Patent: WO2007/56582 A1, 2007 ;
Location in patent: Page/Page column 71 ;
WO 2007/056582 A1
反应条件
hydrogen fluoride
T=70°C; unter Druck;
参考文献
Wiechert
Forschg. Fortschr., 1950 , vol. 26, p. 2. Sonderh. S. 28
反应条件
hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate in water
0.666667 h; Reflux;
参考文献
ABBOTT LABORATORIES; ROCKWAY, Todd W.; BETEBENNER, David A.; DEGOEY, David A.; FLENTGE, Charles A.; HUTCHINSON, Douglas K.; KATI, Warren M.; KRUEGER, Allan C.; LIU, Dachun; LONGENECKER, Kenton L.; PRATT, John K.; STEWART, Kent D.; WAGNER, Rolf
Patent: WO2010/111437 A1, 2010 ;
Location in patent: Page/Page column 77 ;
WO 2010/111437 A1
反应条件
tri(n-propyl)amine; ethanol
参考文献
Cocker; Lapworth; Peters
Journal of the Chemical Society, 1931 , p. 1382,1390
参考文献
Jacobsen
Justus Liebigs Annalen der Chemie, 1871 , vol. 157, p. 245
反应条件
1,1,2,2-tetrachloroethylene; sulfur trioxide
T=0°C;
参考文献
Deutsche Hydrierwerke
Patent: DE846545 , 1944 ;
参考文献
Trillat
Bulletin de la Societe Chimique de France, 1897 , vol. <3>17, p. 230
参考文献
Rebuffat
Gazzetta Chimica Italiana, 1887 , vol. 17, p. 408
参考文献
Trillat
Bulletin de la Societe Chimique de France, 1897 , vol. <3>17, p. 230
