4-苯甲酰基-1-甲烷磺酰基哌啶合成路线 （共 6 条）
反应条件
triethylamine in dichloromethane
T=0 - 20°C; 16 h;
参考文献
ASTRAZENECA AB
Patent: WO2004/56773 A1, 2004 ;
Location in patent: Page 68 ;
WO 2004/056773 A1
反应条件
1: lithium aluminum hydride / tetrahydrofuran / 0 °C
2: pyridinium chlorochromate; Celite / CH2Cl2 / 20 °C
3: tetrahydrofuran / -78 °C
4: pyridinium chlorochromate; Celite / CH2Cl2 / 20 °C
View Scheme
参考文献
Chang, Meng-Yang; Kung, Yung-Hua; Ma, Chih-Chong
Tetrahedron Letters, 2007 , vol. 48, # 2 p. 199 - 202
反应条件
1: tetrahydrofuran / -78 °C
2: pyridinium chlorochromate; Celite / CH2Cl2 / 20 °C
View Scheme
参考文献
Chang, Meng-Yang; Kung, Yung-Hua; Ma, Chih-Chong
Tetrahedron Letters, 2007 , vol. 48, # 2 p. 199 - 202
反应条件
1: pyridinium chlorochromate; Celite / CH2Cl2 / 20 °C
2: tetrahydrofuran / -78 °C
3: pyridinium chlorochromate; Celite / CH2Cl2 / 20 °C
View Scheme
参考文献
Chang, Meng-Yang; Kung, Yung-Hua; Ma, Chih-Chong
Tetrahedron Letters, 2007 , vol. 48, # 2 p. 199 - 202
反应条件
1: triethylamine / CH2Cl2 / 0 °C
2: lithium aluminum hydride / tetrahydrofuran / 0 °C
3: pyridinium chlorochromate; Celite / CH2Cl2 / 20 °C
4: tetrahydrofuran / -78 °C
5: pyridinium chlorochromate; Celite / CH2Cl2 / 20 °C
View Scheme
参考文献
Chang, Meng-Yang; Kung, Yung-Hua; Ma, Chih-Chong
Tetrahedron Letters, 2007 , vol. 48, # 2 p. 199 - 202
反应条件
in dichloromethane
T=0°C;
参考文献
Chang, Meng-Yang; Wu, Tsun-Cheng; Lin, Chun-Yu; Hung, Ching-Yi
Tetrahedron Letters, 2006 , vol. 47, # 47 p. 8347 - 8350
