2-(11-羟基-3-氧代-3H-二苯并[c,h]氧杂蒽-7-基)苯甲酸合成路线 （共 7 条）
反应条件
dihydrogen peroxide in various solvent(s)
T=37°C; pH=7.4;
参考文献
Xu, Kehua; Tang, Bo; Huang, Hui; Yang, Guiwen; Chen, Zhenzhen; Li, Ping; An, Liguo
Chemical Communications, 2005 , # 48 p. 5974 - 5976
反应条件
hydrogen sulfide in aq. phosphate buffer; dimethyl sulfoxide
T=20°C; pH=7.4;
参考文献
Wei, Chao; Zhu, Qing; Liu, Weiwei; Chen, Wenbin; Xi, Zhen; Yi, Long
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 3 p. 479 - 485
反应条件
1: 79 percent / methanesulfonic acid / 12 h / 100 °C
2: 10 percent / pyridine / 20 °C
3: aq. H2O2 / various solvent(s) / 37 °C / pH 7.4
View Scheme
参考文献
Xu, Kehua; Tang, Bo; Huang, Hui; Yang, Guiwen; Chen, Zhenzhen; Li, Ping; An, Liguo
Chemical Communications, 2005 , # 48 p. 5974 - 5976
反应条件
1: 79 percent / methanesulfonic acid / 12 h / 100 °C
2: 10 percent / pyridine / 20 °C
3: aq. H2O2 / various solvent(s) / 37 °C / pH 7.4
View Scheme
参考文献
Xu, Kehua; Tang, Bo; Huang, Hui; Yang, Guiwen; Chen, Zhenzhen; Li, Ping; An, Liguo
Chemical Communications, 2005 , # 48 p. 5974 - 5976
反应条件
1: 10 percent / pyridine / 20 °C
2: aq. H2O2 / various solvent(s) / 37 °C / pH 7.4
View Scheme
参考文献
Xu, Kehua; Tang, Bo; Huang, Hui; Yang, Guiwen; Chen, Zhenzhen; Li, Ping; An, Liguo
Chemical Communications, 2005 , # 48 p. 5974 - 5976
反应条件
methanesulfonic acid
T=135°C; 48 h; Inert atmosphere;
参考文献
Albers, Aaron E.; Dickinson, Bryan C.; Miller, Evan W.; Chang, Christopher J.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 22 p. 5948 - 5950
反应条件
dihydrogen peroxide
T=25°C; pH=7.5; aq. buffer; Kinetics;
参考文献
Albers, Aaron E.; Dickinson, Bryan C.; Miller, Evan W.; Chang, Christopher J.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 22 p. 5948 - 5950
