5-(4-羟苯基)-1H-四唑合成路线 (共 11 条)
反应条件
sodium azide; copper diacetate in N,N-dimethyl-formamide T=120°C; 12 h;
参考文献
Patil, Umakant B.; Kumthekar, Kedar R.; Nagarkar, Jayashree M.
Tetrahedron Letters, 2012 , vol. 53, # 29 p. 3706 - 3709
反应条件
sodium azide in dimethyl sulfoxide T=85°C; 12 h;
参考文献
Shelkar, Radheshyam; Singh, Abhilash; Nagarkar, Jayashree
Tetrahedron Letters, 2013 , vol. 54, # 1 p. 106 - 109
反应条件
HCl (conc.) in toluene
参考文献
Corvas International INC
Patent: US6677473 B1, 2004 ;
US 6677473 B1
反应条件
bismuth trifluoromethanesulphonate; sodium azide; methanecarbohydroxamic acid in N,N-dimethyl-formamide T=120°C; 24 h;
参考文献
Sridhar, Madabhushi; Mallu, Kishore Kumar Reddy; Jillella, Raveendra; Godala, Kondalreddy; Beeram, Chinaramanaiah; Chinthala, Narsaiah
Synthesis (Germany), 2013 , vol. 45, # 4 art. no. SS-2012-Z0887-OP, p. 507 - 510
反应条件
T=530°C; P=0.03 Torr; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 61, # 13 p. 4460 - 4461
反应条件
T=620°C; P=1.8 Torr; other temperature, pressure; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 61, # 13 p. 4462 - 4465
反应条件
T=620°C; P=1.8 Torr; other temperature, pressure; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 61, # 13 p. 4462 - 4465
反应条件
T=530°C; P=0.03 Torr; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 61, # 13 p. 4460 - 4461
反应条件
T=620°C; P=1.8 Torr; other temperature, pressure; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 61, # 13 p. 4462 - 4465
反应条件
T=530°C; P=0.03 Torr; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 61, # 13 p. 4460 - 4461