Franks, Stephen; Hartley, Frank R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2233 - 2237
potassium hydroxide; hydrazine hydrate in diethylene glycol 130 deg C, 2 h then 200 deg C, 2 h;
参考文献
Gray, George W.; Hird, Michael; Lacey, David; Toyne, Kenneth J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 2041 - 2054
1: 98 percent / diethyl ether / 0 °C 2: NaI / acetonitrile / 12 h / 20 °C 3: 21.52 g / NaBH4 / dimethylsulfoxide / 12 h / 20 °C View Scheme
参考文献
Franks, Stephen; Hartley, Frank R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2233 - 2237
1: NaI / acetonitrile / 12 h / 20 °C 2: 21.52 g / NaBH4 / dimethylsulfoxide / 12 h / 20 °C View Scheme
参考文献
Franks, Stephen; Hartley, Frank R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2233 - 2237
1: 98 percent / aluminum chloride / 0 deg C, 1 h then 80 deg C, 2 h 2: 40 percent / hydrazine hydrate, potassium hydroxide / bis-(2-hydroxy-ethyl) ether / 130 deg C, 2 h then 200 deg C, 2 h View Scheme
参考文献
Gray, George W.; Hird, Michael; Lacey, David; Toyne, Kenneth J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 2041 - 2054
1: 98 percent / aluminum chloride / 0 deg C, 1 h then 80 deg C, 2 h 2: 40 percent / hydrazine hydrate, potassium hydroxide / bis-(2-hydroxy-ethyl) ether / 130 deg C, 2 h then 200 deg C, 2 h View Scheme
参考文献
Gray, George W.; Hird, Michael; Lacey, David; Toyne, Kenneth J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 2041 - 2054
