1-(6-甲基-2-萘基)乙酮合成路线 (共 10 条)
反应条件
pyridine; water; iodine in methanol T=30°C; other temperatures; ΔH(excit.); KineticsMechanismThermodynamic data;
参考文献
Ananthakrishnanadar, P.; Gnanasekaran, C.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1980 , vol. 19, # 7 p. 646 - 649
反应条件
dihydrogen peroxide; acetic anhydride; acetic acid in formic acid; water
参考文献
Mitsubishi Gas Chemical Company, Inc.
Patent: US4801737 A1, 1989 ;
反应条件
hydrogenchloride; amalgamated zinc; ethanol
参考文献
Kon; Weller
Journal of the Chemical Society, 1939 , p. 792
反应条件
1: 55 percent / NBS, benzoyl peroxide / CCl4 / Heating
2: 50 percent / ethanol / 8 h / Heating
3: 50 percent / KOH, water / 2-methoxy-ethanol / 48 h / 100 °C
View Scheme
参考文献
Saint Martino Descours; Pacheco; Venco; Yavordios
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 1 p. 5 - 9
反应条件
sodium hydroxide; bromine in water
2 h; Ambient temperature;
参考文献
Friese, V.; Boos, A.; Bauch, H.-J.; Leistner, E.
Phytochemistry (Elsevier), 1993 , vol. 32, # 3 p. 613 - 622
反应条件
pyridine; water; iodine in methanol
T=30°C; other temperatures; ΔH(excit.); KineticsMechanismThermodynamic data;
参考文献
Ananthakrishnanadar, P.; Gnanasekaran, C.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1980 , vol. 19, # 7 p. 646 - 649
反应条件
KBrO3; water; potassium bromide in ethanol
0.75 h;
参考文献
Thirunarayanan; Vanangamudi; Sathiyendran; Ravi
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2011 , vol. 50, # 4 p. 593 - 604
反应条件
1: KBrO3; water; potassium bromide / ethanol / 0.75 h
2: water / ethanol / 4 h / Reflux
View Scheme
参考文献
Thirunarayanan; Vanangamudi; Sathiyendran; Ravi
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2011 , vol. 50, # 4 p. 593 - 604
反应条件
T=470 - 510°C; drip type pyrrolysis unit filled with fine Vycor chips was used; Yield given;
参考文献
Zoeller, Joseph R. Tetrahedron Letters, 1989 , vol. 30, # 12 p. 1457 - 1460
反应条件
in nitrobenzene (acetylation);
参考文献
Wells,P.R.; Alcorn,P.G.E. Australian Journal of Chemistry, 1963 , vol. 16, p. 1108 - 1118