1,4-二碘-2,3-二甲氧基苯合成路线 （共 5 条）
反应条件
boron tribromide in dichloromethane T=20°C; 14 h;
参考文献
Zhao, Yan-Li; Liu, Lihua; Zhang, Wenyu; Sue, Chi-Hau; Li, Qiaowei; Miljanic, Ognjen S.; Yaghi, Omar M.; Fraser Stoddart
Chemistry - A European Journal, 2009 , vol. 15, # 48 p. 13356 - 13380
反应条件
1: 90 percent / BBr3 / CH2Cl2 / 14 h / 20 °C
2: 96 percent / K2CO3 / dimethylformamide / 5 h / 120 °C
View Scheme
参考文献
Zhu, Zhengguo; Swager, Timothy M.
Organic Letters, 2001 , vol. 3, # 22 p. 3471 - 3474
反应条件
iodine cloride in dichloromethane
T=0 - 20°C;
参考文献
Weibel, Nicolas; Mishchenko, Artera; Wandlowski, Thomas; Neuburger, Markus; Leroux, Yann; Mayor, Marcel
European Journal of Organic Chemistry, 2009 , # 35 p. 6140 - 6150
反应条件
(i) nBuLi, Me2NCH2CH2NMe2, heptane, hexane, (ii) I2; Multistep reaction;
参考文献
Pring,B.G.
Acta Chemica Scandinavica (1947-1973), 1973 , vol. 27, p. 3873 - 3880
反应条件
1.1: n-BuLi; TMEDA / hexane / 25 h / 20 °C
1.2: 89 percent / hexane / 5 h / -78 - 20 °C
2.1: 80.9 percent / ICl / CH2Cl2 / 0.5 h / 20 °C
View Scheme
参考文献
Zhu, Zhengguo; Swager, Timothy M.
Organic Letters, 2001 , vol. 3, # 22 p. 3471 - 3474
