3,7-二甲基-6-辛烯腈合成路线 （共 10 条）
反应条件
2,3'-bipyridine; ammonium hydroxide; copper(l) iodide; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; oxygen in acetonitrile T=50°C; 24 h;
参考文献
Yin, Weiyu; Wang, Chengming; Huang, Yong
Organic Letters, 2013 , vol. 15, # 8 p. 1850 - 1853
反应条件
2,4,6-trichloro-1,3,5-triazine in N,N-dimethyl-formamide T=20°C; Beckmann rearrangement; 4 h;
参考文献
De Luca, Lidia; Giacomelli, Giampaolo; Porcheddu, Andrea
Journal of Organic Chemistry, 2002 , vol. 67, # 17 p. 6272 - 6274
反应条件
sodium tetrahydroborate; RuCl3 monohydrate in 1-methyl-pyrrolidin-2-one; water T=0°C; 1 h; chemoselective reaction;
参考文献
Babler, James H.; Ziemke, David W.; Hamer, Robert M.
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1754 - 1757
反应条件
ammonium hydroxide; dihydrogen peroxide; copper dichloride in isopropyl alcohol T=17 - 30°C; oxidative dehydrogenation;
参考文献
Erman; Snow; Williams
Tetrahedron Letters, 2000 , vol. 41, # 35 p. 6749 - 6752
反应条件
(μ3,η2,η3,η5-acenaphthylene)Ru3(CO)7; 1,1,4,4-tetramethyldisilylethylene in ethylene glycol dimethyl ether T=80°C; 20 h; Inert atmosphere;
参考文献
Hanada, Shiori; Motoyama, Yukihiro; Nagashima, Hideo
European Journal of Organic Chemistry, 2008 , # 24 p. 4097 - 4100
反应条件
carbon disulfide; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in benzene 20 h; Ambient temperature;
参考文献
Shinozaki, Hiraku; Imaizumi, Mari; Tajima, Moritaka
Chemistry Letters, 1983 , p. 929 - 932
反应条件
magnesium in methanol
参考文献
Profitt,J.A. et al.
Journal of Organic Chemistry, 1975 , vol. 40, # 1 p. 127 - 128
反应条件
hydrogen; palladium on activated carbon in water T=50 - 81°C; P=3750.38 - 37503.8 Torr; 4.83333 - 6 h; Product distribution / selectivity;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2006/106141 A1, 2006 ;
Location in patent: Page/Page column 10-11 ;
反应条件
hydrogen; nickel T=40 - 50°C; P=7500.75 - 22502.3 Torr; 12 h; Product distribution / selectivity;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2006/106141 A1, 2006 ;
Location in patent: Page/Page column 12 ;
反应条件
Raney Co; ammonia; hydrogen in methanol T=100°C; P=60004.8 Torr; Product distribution; Further Variations:Reagents;
参考文献
Kukula, Pavel; Koprivova, Klara
Journal of Catalysis, 2005 , vol. 234, # 1 p. 161 - 171
