1-(4-苄氧基-3-硝基)苯基环氧乙烷合成路线 (共 6 条)
反应条件
sodium hydroxide in water
参考文献
Pharmacia AS
Patent: US4072760 A1, 1978 ;
反应条件
sodium hydroxide; sodium tetrahydroborate 1.) MeOH; Multistep reaction;
参考文献
Mereyala, Hari Babu; Sambaru, Kalyani
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 1 p. 167 - 169
反应条件
1: TBAI, K2CO3 / acetone 2: Br2 / CHCl3 3: 1.) NaBH4 2.) NaOH / 1.) MeOH View Scheme
参考文献
Mohan, K. Chandra; Ravikumar, K.; Vittal, T. V. S. K.; Gido, C. K.
Acta Crystallographica, Section C: Crystal Structure Communications, 1994 , vol. 50, # 8 p. 1294 - 1295
反应条件
1: Br2 / CHCl3 2: 1.) NaBH4 2.) NaOH / 1.) MeOH View Scheme
参考文献
Mohan, K. Chandra; Ravikumar, K.; Vittal, T. V. S. K.; Gido, C. K.
Acta Crystallographica, Section C: Crystal Structure Communications, 1994 , vol. 50, # 8 p. 1294 - 1295
反应条件
1: HNO3 / acetic acid / 0 °C 2: TBAI, K2CO3 / acetone 3: Br2 / CHCl3 4: 1.) NaBH4 2.) NaOH / 1.) MeOH View Scheme
参考文献
Mohan, K. Chandra; Ravikumar, K.; Vittal, T. V. S. K.; Gido, C. K.
Acta Crystallographica, Section C: Crystal Structure Communications, 1994 , vol. 50, # 8 p. 1294 - 1295
反应条件
1: HOAc / methanol
2: 10.6 g / triphenylphosphine; imidazole; iodine / toluene / 3 h / Heating
View Scheme
参考文献
Mereyala, Hari Babu; Sambaru, Kalyani
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 1 p. 167 - 169