1-羟基-2-苯甲酸丙酯合成路线 (共 14 条)
反应条件
potassium permanganate; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane; water
4 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Nai-ju, Huang; Liang-heng, Xu
Synthetic Communications, 1990 , vol. 20, # 10 p. 1563 - 1567
反应条件
tert.-butylhydroperoxide; potassium carbonate; 1-tert-butylperoxy-1,2-benziodoxol-3(1H)-one in benzene
T=20°C; 36 h;
参考文献
Sueda, Takuya; Fukuda, Sonoko; Ochiai, Masahito
Organic Letters, 2001 , vol. 3, # 15 p. 2387 - 2390
反应条件
lithium boron tetrafluoride in dichloromethane; acetonitrile
T=20°C;
参考文献
Santaniello, Enzo; Casati, Silvana; Ciuffreda, Pierangela; Gamberoni, Luca
Tetrahedron Asymmetry, 2005 , vol. 16, # 9 p. 1705 - 1708
反应条件
potassium carbonate
T=175°C; P=75007.5 Torr; 62 h; Reagent/catalystSolventConcentrationPressure;
参考文献
Da Silva; Dayoub; Mignani; Raoul; Lemaire
Catalysis Communications, 2012 , vol. 29, p. 58 - 62
反应条件
1: 85 percent / Et3N / CH2Cl2 / 0.33 h
2: Et3N / CH2Cl2 / 24 h / Ambient temperature
View Scheme
参考文献
Kim, Sunggak; Chang, Heung; Kim, Wan Joo
Journal of Organic Chemistry, 1985 , vol. 50, # 10 p. 1751 - 1752
反应条件
EPPS buffer; lanthanum trifluoromethanesulphonate in water
T=25°C; pH=7; Kinetics;
参考文献
Cameron, Lisa L.; Wang, Sheila C.; Kluger, Ronald
Journal of the American Chemical Society, 2004 , vol. 126, # 34 p. 10721 - 10726
反应条件
aluminum oxide; methanesulfonic acid
T=80°C; 4.5 h;
参考文献
Sharghi, Hashem; Sarvari, Mona Hosseini
Journal of Organic Chemistry, 2003 , vol. 68, # 10 p. 4096 - 4099
反应条件
triethylamine in dichloromethane
24 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kim, Sunggak; Chang, Heung; Kim, Wan Joo
Journal of Organic Chemistry, 1985 , vol. 50, # 10 p. 1751 - 1752
反应条件
aluminum oxide; methanesulfonic acid
T=80°C; 0.583333 h;
参考文献
Sharghi, Hashem; Sarvari, Mona Hosseini
Tetrahedron, 2003 , vol. 59, # 20 p. 3627 - 3633
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
0.333333 h; Ambient temperature; Product distribution;
参考文献
Sekine, Mitsuo; Kume, Akiko; Hata, Tsujiaki
Tetrahedron Letters, 1981 , vol. 22, # 37 p. 3617 - 3620