N1-丁基苯-1,2-二胺合成路线 （共 9 条）
参考文献
Ralph, J. T.
Synthetic Communications, 1989 , vol. 19, # 7,8 p. 1381 - 1388
反应条件
hydrogenchloride; sodium nitrite
参考文献
Journal of the Chemical Society, , p. 4559,4561
反应条件
Oxonereg; in water; N,N-dimethyl-formamide
T=20°C; 12 h;
参考文献
Blatch, Alexandrea J.; Chetina, Olga V.; Howard, Judith A.K.; Patrick, Leonard G.F.; Smethurst, Christian A.; Whiting, Andrew
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 17 p. 3297 - 3302
参考文献
UNIVERSITY OF DURHAM
Patent: WO2004/113351 A2, 2004 ;
Location in patent: Page 28-29 ;
反应条件
hydrogenchloride; tin
1 h; Heating;
参考文献
Beger, J.; Wagner, G.; Uhlig, E.; Dinjus, U.
Journal fuer Praktische Chemie (Leipzig), 1983 , vol. 325, # 5 p. 708 - 718
反应条件
1: in dichloromethane
T=50°C; P=7500600 Torr; 5 h;
2: With hydrogenchloride in water
0.166667 h;
参考文献
Agafonov; Dudin; Preobrazhenskii; Zhulin
Russian Chemical Bulletin, 2003 , vol. 52, # 1 p. 273 - 275
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C; 4 h;
参考文献
Xue, Ding; Long, Ya-Qiu
Journal of Organic Chemistry, 2014 , vol. 79, # 10 p. 4727 - 4734
反应条件
1: 62 percent / nitrobenzene / 6 h / 190 - 200 °C
2: 50 percent / Sn, halfconc. HCl / 1 h / Heating
View Scheme
参考文献
Beger, J.; Wagner, G.; Uhlig, E.; Dinjus, U.
Journal fuer Praktische Chemie (Leipzig), 1983 , vol. 325, # 5 p. 708 - 718
参考文献
Ralph, J. T.
Synthetic Communications, 1989 , vol. 19, # 7,8 p. 1381 - 1388
