N-亚苄基-4-甲基苯磺酰胺合成路线 （共 129 条）
反应条件
(η5-C5Ph5)Ru(CO)2Cl; potassium tert-butylate in tetrahydrofuran; toluene
T=40°C; Mannich type reaction; 15 h; Inert atmosphereMolecular sieve; optical yield given as percent dediastereoselective reaction;
参考文献
Bartoszewicz, Agnieszka; Jezowska, Martina M.; Laymand, Kevin; Moebus, Juri; Martin-Matute, Belen
European Journal of Inorganic Chemistry, 2012 , # 9 p. 1517 - 1530
反应条件
in dimethyl sulfoxide
T=100°C; 12 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Fang, Fan; Li, Yuan; Tian, Shi-Kai
European Journal of Organic Chemistry, 2011 , # 6 p. 1084 - 1091
反应条件
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene in tetrahydrofuran; water
T=20°C; Pinnick oxidation; 8 h;
参考文献
Mohamed, Magdi A.; Yamada, Ken-ichi; Tomioka, Kiyoshi
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3436 - 3438
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate in isopropyl alcohol
T=75°C; Michael Addition; 12 h; Schlenk techniqueSealed tubeInert atmosphere;
参考文献
Jin, Zhichao; Xu, Jianfeng; Yang, Song; Song, Bao-An; Chi, Yonggui Robin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 47 p. 12354 - 12358
Angew. Chem., 2013 , vol. 125, # 47 p. 12580 - 12584,5
反应条件
potassium tert-butylate in tert-butyl alcohol
T=50°C; tandem Knoevenagel-Michael addition; 4 h;
参考文献
Fan, Renhua; Wang, Weizi; Pu, Dongming; Wu, Jie
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5905 - 5907
反应条件
potassium tert-butylate in tert-butyl alcohol
T=50°C;
参考文献
Fan, Renhua; Wang, Weizi; Pu, Dongming; Wu, Jie
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5905 - 5907
反应条件
1: 18 percent / t-BuOK / 2-methyl-propan-2-ol / 50 °C
2: 85 percent / t-BuOK / 2-methyl-propan-2-ol / 50 °C
3: 92 percent / t-BuOK / 2-methyl-propan-2-ol / 50 °C
View Scheme
参考文献
Fan, Renhua; Wang, Weizi; Pu, Dongming; Wu, Jie
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5905 - 5907
反应条件
[Cp*Rh(CH3CN)3](SbF6)2; copper (II) acetate monohydrate; acetic acid in 1,4-dioxane
T=80°C; 14 h; Inert atmosphere;
参考文献
Zhang, Tao; Wu, Lamei; Li, Xingwei
Organic Letters, 2013 , vol. 15, # 24 p. 6294 - 6297
反应条件
1: [{(η5-C5Me5)RhCl}2(μ-Cl)2]; AgB(C6F5)4 / 1,2-dichloro-ethane / 16 h / 75 °C / Inert atmosphere
2: toluene-4-sulfonic acid / toluene / 16 h / 100 °C
3: methanol; naphthalene; sodium / ethylene glycol dimethyl ether / 2.08 h / -78 - 20 °C / Inert atmosphere
View Scheme
参考文献
Hesp, Kevin D.; Bergman, Robert G.; Ellman, Jonathan A.
Organic Letters, 2012 , vol. 14, # 9 p. 2304 - 2307
反应条件
chloro-trimethyl-silane; bismuth sulphate in dichloromethane
T=20°C; Friedel-Crafts reaction; 5 h;
参考文献
Liu, Cong-Rong; Li, Man-Bo; Yang, Cui-Feng; Tian, Shi-Kai
Chemical Communications, 2008 , # 10 p. 1249 - 1251
