N-亚苄基-4-甲基苯磺酰胺合成路线 (共 129 条)
反应条件
diethylzinc in toluene T=50°C; 24 h;
参考文献
Zani, Lorenzo; Alesi, Silvia; Cozzi, Pier Giorgio; Bolm, Carsten
Journal of Organic Chemistry, 2006 , vol. 71, # 4 p. 1558 - 1562
参考文献
Organic Letters, , vol. 4, # 20 p. 3509 - 3511
参考文献
Organic Letters, , vol. 4, # 20 p. 3509 - 3511
反应条件
copper(II) bis(trifluoromethanesulfonate); (S)-1-[2-diphenylphosphinomethyl-4,4-bis(2,4,6-triisopropylphenylmethyl)pyrrolidin-1-yl]-2,2-dimethylpropan-1-one in hexane; toluene T=0°C; 0 h; Title compound not separated from byproducts;
参考文献
Soeta, Takahiro; Nagai, Kazushige; Fujihara, Hidetaka; Kuriyama, Masami; Tomioka, Kiyoshi
Journal of Organic Chemistry, 2003 , vol. 68, # 25 p. 9723 - 9727
反应条件
[(Cp*Ir)2(μ-NTs)2]; potassium tert-butylate in toluene 17 h; Inert atmosphereReflux;
参考文献
Organic Letters, , vol. 12, # 6 p. 1336 - 1339
反应条件
1: diethylzinc With chiral amidophosphine; copper(II) bis(trifluoromethanesulfonate) in toluene T=20°C; 0.333333 h; 2: N-benzylidene-4-methylbenzenesulfonamide T=0°C; 3 h;
参考文献
Nagai, Kazushige; Fujihara, Hidetaka; Kuriyama, Masami; Yamada, Ken-ichi; Tomioka, Kiyoshi
Chemistry Letters, 2002 , # 1 p. 8 - 9
反应条件
air; boron trifluoride diethyl etherate T=20°C; 54 h;
参考文献
Tetrahedron Letters, , vol. 45, # 35 p. 6595 - 6597
反应条件
Cs2CO3; catalyst: PPh3 in tetrahydrofuran; methanol ligand and B comps. (1:1.2 molar ratio) at 70°C for 15 h; NMR;
参考文献
Sole, Cristina; Gulyas, Henrik; Fernandez, Elena
Chemical Communications, 2012 , vol. 48, # 31 p. 3769 - 3771
反应条件
[bis(acetoxy)iodo]benzene; potassium tert-butylate; tetrabutylammomium bromide in acetonitrile T=0 - 30°C;
参考文献
Fan, Renhua; Ye, Yang
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 10 p. 1526 - 1530
反应条件
1: With methyllithium in tetrahydrofuran; diethyl ether T=-78°C; 3 h; Inert atmosphere; 2: With water; ammonium chloride in tetrahydrofuran; diethyl ether T=-78°C;
参考文献
Concellon, Jose M.; Rodriguez-Solla, Humberto; Bernad, Pablo L.; Simal, Carmen
Journal of Organic Chemistry, 2009 , vol. 74, # 6 p. 2452 - 2459