N-亚苄基-4-甲基苯磺酰胺合成路线 （共 129 条）
反应条件
tri(isobutyl)phosphine in toluene
T=120°C; 5 h; Inert atmosphere;
参考文献
Panossian, Armen; Fleury-Bregeot, Nicolas; Marinetti, Angela
European Journal of Organic Chemistry, 2008 , # 22 p. 3826 - 3833
反应条件
in tetrahydrofuran
T=20°C;
参考文献
Wu, Chao; Huang, Wangyong; He, Weimin; Xiang, Jiannan
Chemistry Letters, 2013 , vol. 42, # 10 p. 1233 - 1234
反应条件
copper diacetate; potassium carbonate
T=150°C; 3 h;
参考文献
Cui, Xinjiang; Shi, Feng; Tse, Man Kin; Goerdes, Dirk; Thurow, Kerstin; Beller, Matthias; Deng, Youquan
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 17 p. 2949 - 2958
反应条件
air; copper diacetate; potassium carbonate
T=150°C; 3 h; Mechanism;
参考文献
Cui, Xinjiang; Shi, Feng; Zhang, Yan; Deng, Youquan
Tetrahedron Letters, 2010 , vol. 51, # 15 p. 2048 - 2051
反应条件
FeCl3·6H2O in dichloromethane
T=20°C; Friedel Crafts arylation; 2.5 h; Inert atmosphere;
参考文献
Thirupathi, Ponnaboina; Soo Kim, Sung
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 5240 - 5249
反应条件
in acetonitrile
T=25°C; 48 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Fang, Fan; Li, Yuan; Tian, Shi-Kai
European Journal of Organic Chemistry, 2011 , # 6 p. 1084 - 1091
反应条件
in acetonitrile
T=25°C; 24 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Fang, Fan; Li, Yuan; Tian, Shi-Kai
European Journal of Organic Chemistry, 2011 , # 6 p. 1084 - 1091
反应条件
in toluene
T=25°C; 24 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Fang, Fan; Li, Yuan; Tian, Shi-Kai
European Journal of Organic Chemistry, 2011 , # 6 p. 1084 - 1091
反应条件
1: 77 percent / LDA / hexane; tetrahydrofuran / 1.) -78 to 0 deg C, 45 min; 25 deg C, 3 h, 2.) -78 deg C, 5 min; -78 to 0 deg C
2: 98 percent / Br2 / CH2Cl2; CCl4 / 3 h / 25 °C
3: 99 percent / NaH / tetrahydrofuran; paraffin / 1.) 0 deg C, 10 min; 0 to 25 deg C, 10 min, 2.) reflux, 2 h
4: 85 percent / p-TsOH, molecular sieves 4 Angstroem / toluene / 4 h / Heating
5: 48 percent / n-BuLi / tetrahydrofuran; hexane / 1.) 0 deg C, 10 min, 2.) reflux, 3 h
View Scheme
参考文献
Love, Brian E.; Raje, Prasad S.
Journal of Organic Chemistry, 1994 , vol. 59, # 11 p. 3219 - 3222
反应条件
potassium fluoride; (η3-allyl)(η5-Cp)Pd in N,N-dimethyl-formamide
T=100°C; 3 h;
参考文献
Ueno, Satoshi; Ohtsubo, Masakazu; Kuwano, Ryoichi
Journal of the American Chemical Society, 2009 , vol. 131, # 36 p. 12904 - 12905
