反应条件
1: benzaldehyde Schiff base of glycine methyl ester With n-butyllithium; diisopropylamine in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; hexane T=-60°C; Metallation; 1 h; 2: 4-bromo-but-1-ene in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; hexane T=20°C; Alkylation; Further stages.;
参考文献
Blaauw, Rolf; Kingma, Irene E.; Laan, Jan H.; Van Der Baan, Juul L.; Balt, Sijbe; De Bolster, Martinus W. G.; Klumpp, Gerhard W.; Smeets, Wilberth J. J.; Spek, Anthony L.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 8 p. 1199 - 1210