反应条件
1: 95 percent / p-toluenesulfonic acid / CH2Cl2 / 0.5 h 2: 79 percent / diisobutylaluminum hydride / toluene; hexane / 0.33 h 3: 1.) sodium methylsulfinylcarbanide / 1.) Me2SO, 2.) Me2SO, 2 h 4: Jones reagent / acetone / 0.08 h / -20 °C 5: 43 percent / 65percent aq. acetic acid / 14 h View Scheme
参考文献
Tolstikov, G. A.; Adler, M. E.; Miftakhov, M. S.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 101 p. 1908 - 1914
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 10 p. 2113 - 2119
