2-乙基1-(2-甲基-2-丙基)4-溴-1H-吡咯-1,2-二羧酸酯合成路线 （共 6 条）
反应条件
in N,N-dimethyl-formamide T=120°C; 6 h;
参考文献
Handy, Scott T.; Bregman, Howard; Lewis, Jennifer; Zhang, Xiaolei; Zhang, Yanan
Tetrahedron Letters, 2003 , vol. 44, # 3 p. 427 - 430
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in water; N,N-dimethyl-formamide T=110°C; Suzuki coupling; 15 h;
参考文献
Handy, Scott T.; Zhang, Yanan; Bregman, Howard
Journal of Organic Chemistry, 2004 , vol. 69, # 7 p. 2362 - 2366
反应条件
1: 100 percent / dimethylformamide / 6 h / 120 °C 2: 80 percent / aq. Na2CO3 / palladium tetrakis-triphenylphosphine / dimethylformamide / 14 h / 110 °C View Scheme
参考文献
Handy, Scott T.; Bregman, Howard; Lewis, Jennifer; Zhang, Xiaolei; Zhang, Yanan
Tetrahedron Letters, 2003 , vol. 44, # 3 p. 427 - 430
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=110°C; Suzuki-type coupling;
参考文献
Tetrahedron Letters, , vol. 44, # 3 p. 427 - 430
反应条件
1: 100 percent / dimethylformamide / 6 h / 120 °C 2: 28 percent / aq. Na2CO3 / palladium tetrakis-triphenylphosphine / dimethylformamide / 110 °C View Scheme
参考文献
Handy, Scott T.; Bregman, Howard; Lewis, Jennifer; Zhang, Xiaolei; Zhang, Yanan
Tetrahedron Letters, 2003 , vol. 44, # 3 p. 427 - 430
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile
T=20°C; 1 h;
参考文献
Handy, Scott T.; Zhang, Yanan; Bregman, Howard
Journal of Organic Chemistry, 2004 , vol. 69, # 7 p. 2362 - 2366
