5-甲基-3-己烯-2-酮合成路线 （共 29 条）
反应条件
toluene-4-sulfonic acid in 1,4-dioxane T=110°C; 0.0130556 h;
参考文献
Tanaka, Katsunori; Motomatsu, Shinya; Koyama, Koichi; Tanaka, Shin-Ichi; Fukase, Koichi
Organic Letters, 2007 , vol. 9, # 2 p. 299 - 302
反应条件
RuCl3H(p-cymene)2; immobilized lipase from Pseudomonas cepacia; triethylamine in dichloromethane T=20 - 25°C; Acetylation; oxidation; reduction; 48 h; Enzymatic reaction;
参考文献
Lee; Huh; Kim; Jung; Koh; Park
Organic letters, 2000 , vol. 2, # 15 p. 2377 - 2379
反应条件
sodium hydroxide; sulfuric acid in chloroform; water; acetoacetic acid methyl ester
参考文献
Nippon Soda Co., Ltd.
Patent: US5484949 A1, 1996 ;
反应条件
piperidine; acetic acid
参考文献
Brophy, Peter M.; Campbell, Alison M.; Van Eldik, Annamaria J.; Teesdale-Spittle, Paul H.; Liebau, Eva; Wang, Meng F.
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 9 p. 979 - 981
反应条件
L-proline T=20°C; 48 h;
参考文献
Dodda, Rajasekhar; Zhao, Cong-Gui
Synthesis, 2006 , # 19 p. 3238 - 3242
反应条件
potassium tert-butylate in tert-butyl alcohol
参考文献
Muir,D.M.; Parker,A.J.
Journal of Organic Chemistry, 1976 , vol. 41, p. 3201 - 3204
反应条件
titanium tetrachloride in dichloromethane T=-78°C; Yield given. Yields of byproduct given;
参考文献
Ivashchenko, N. B.; Polunin, E. V.; Kashin, A. N.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 4 p. 546 - 550
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 4 p. 512 - 516
反应条件
in dimethyl sulfoxide T=30°C; ΔGchem, other solvent, other temp.; Equilibrium constantThermodynamic data;
参考文献
Hine, Jack; Linden, Shwn-Meei
Journal of Organic Chemistry, 1983 , vol. 48, # 4 p. 584 - 587
反应条件
sulfuric acid Heating;
参考文献
Muir,D.M.; Parker,A.J.
Journal of Organic Chemistry, 1976 , vol. 41, p. 3201 - 3204
参考文献
Bertrand,M.; Le Gras,J.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1965 , vol. 261, p. 762 - 765
