甘醇钠二硫加成化合物的水合物合成路线 （共 52 条）
反应条件
acetic acid und Erhitzen des Reaktionsprodukts auf 240grad/15 Torr;
参考文献
Koenigs; Bueren; Jung
Chemische Berichte, 1936 , vol. 69, p. 2691
参考文献
Chambers, Richard D.; Parsons, Mandy; Sandford, Graham; Skinner, Christopher J.; Atherton, Malcolm J.; Moilliet, John S.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 7 p. 803 - 810
反应条件
in water 0.75 h; RefluxInert atmosphere;
参考文献
Wang, Jingjing; Zuo, Sujing; Chen, Weiqiang; Zhang, Xinrui; Tan, Kaixin; Tian, Yun; Wang, Jianhui
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8217 - 8231
反应条件
1: in ethanol; water T=40°C; 0.5 h; 2: With sodium hydroxide; water in ethanol T=40 - 60°C; pH=12 - 13; 4 h; 3: With hydrogenchloride; water in ethanol pH=1 - 2;
参考文献
Conte, Aurelia; Dehmlow, Henrietta; Grether, Uwe; Kratochwil, Nicole A.; Kuehne, Holger; Narquizian, Robert; Panousis, Constantinos G.; Peters, Jens-Uwe; Ricklin, Fabienne
Patent: US2008/234277 A1, 2008 ;
Location in patent: Page/Page column 18 ;
US 20080234277 A1
参考文献
Hinsberg; Rosenzweig
Chemische Berichte, 1894 , vol. 27, p. 3254
参考文献
Scapecchi, Serena; Martini, Elisabetta; Manetti, Dina; Ghelardini, Carla; Martelli, Cecilia; Dei, Silvia; Galeotti, Nicoletta; Guandalini, Luca; Romanelli, Maria Novella; Teodori, Elisabetta
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 1 p. 71 - 85
参考文献
Chambers, Richard D.; Parsons, Mandy; Sandford, Graham; Skinner, Christopher J.; Atherton, Malcolm J.; Moilliet, John S.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 7 p. 803 - 810
反应条件
1: With water T=60 - 75°C; 1 h; 2: With sodium hydroxide in water pH=7.5 - 7.8;
参考文献
Wyeth
Patent: US2005/282820 A1, 2005 ;
Location in patent: Page/Page column 17-18 ;
US 20050282820 A1
反应条件
sodium acetate; acetic acid
参考文献
Cavagnol; Wiselogle
Journal of the American Chemical Society, 1947 , vol. 69, p. 795,796
反应条件
sodium carbonate in 1,4-dioxane 0.916667 h;
参考文献
Mokhtar, Hassan M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 268 - 272
