N,N,N’,N’-四甲基-1,6-己二胺合成路线 （共 10 条）
反应条件
hydrogen; platinum(IV) oxide in acetic acid
T=25°C; P=73550.8 Torr; 24 h;
参考文献
Winiker, Robert; Beckhaus, Hans-Dieter; Ruechardt, Christoph
Chemische Berichte, 1980 , vol. 113, # 11 p. 3456 - 3476
反应条件
sodium naphthalenide
参考文献
Sargent,G.D.; Lux,G.A.
Journal of the American Chemical Society, 1968 , vol. 90, p. 7160 - 7162
反应条件
1: 68 percent / MeLi / diethyl ether / 1) 1 h, reflux, 2) overnight, r.t.
2: 54 percent / H2 / PtO2 / acetic acid / 24 h / 25 °C / 73550.8 Torr
View Scheme
参考文献
Winiker, Robert; Beckhaus, Hans-Dieter; Ruechardt, Christoph
Chemische Berichte, 1980 , vol. 113, # 11 p. 3456 - 3476
反应条件
lithium in tetrahydrofuran
T=20°C; Wurtz reaction; Inert atmosphereSonication;
参考文献
Vandenburg, Daniel; Price, Gareth J.
Ultrasonics Sonochemistry, 2012 , vol. 19, # 1 p. 5 - 8
反应条件
mercury
HeatingIrradiation;
参考文献
Brown, Stephen H.; Crabtree, Robert H.
Journal of the American Chemical Society, 1989 , vol. 111, # 8 p. 2935 - 2946
反应条件
mercury
17 h; HeatingIrradiationother alkanes; selectivity of cross-dimerization, relative reactivities in cross-dimerizations; Product distributionMechanism;
参考文献
Brown, Stephen H.; Crabtree, Robert H.
Journal of the American Chemical Society, 1989 , vol. 111, # 8 p. 2946 - 2953
反应条件
mercury
1 h; HeatingIrradiation;
参考文献
Brown, Stephen H.; Crabtree, Robert H.
Journal of the American Chemical Society, 1989 , vol. 111, # 8 p. 2935 - 2946
反应条件
mercury
17 h; HeatingIrradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Brown, Stephen H.; Crabtree, Robert H.
Journal of the American Chemical Society, 1989 , vol. 111, # 8 p. 2946 - 2953
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; carbon monoxide in diethyl ether
参考文献
Sprangers,W.J.J.M.; Louw,R.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1976 , p. 1895 - 1901
参考文献
Howard et al.
Journal of Research of the National Bureau of Standards (United States), vol. 38, p. 388,390
Chem.Abstr., 1947 , p. 5291
