jones reagent in acetone ice bath;

1: 74.1 percent / sodium methoxide / benzene / 1 h / Heating 2: 63.7 percent / NBS, BPO / CCl4 / 2 h / Heating 3: 96.5 percent / water / nitromethane / 2 h / Heating 4: 95.4 percent / Jones reagent / acetone / ice bath View Scheme

1: 96.5 percent / water / nitromethane / 2 h / Heating 2: 95.4 percent / Jones reagent / acetone / ice bath View Scheme

1: 74.1 percent / sodium methoxide / benzene / 1 h / Heating 2: 63.7 percent / NBS, BPO / CCl4 / 2 h / Heating 3: 96.5 percent / water / nitromethane / 2 h / Heating 4: 95.4 percent / Jones reagent / acetone / ice bath View Scheme

1: 63.7 percent / NBS, BPO / CCl4 / 2 h / Heating 2: 96.5 percent / water / nitromethane / 2 h / Heating 3: 95.4 percent / Jones reagent / acetone / ice bath View Scheme