顺-二环[3.3.0]辛烷-3,7-二酮合成路线 （共 16 条）
参考文献
Knotnerus,J.; Bickel,A.F.
Recueil des Travaux Chimiques des Pays-Bas, 1964 , vol. 83, p. 400 - 413
反应条件
sulfuric acid in water T=10 - 15°C; 3 h;
参考文献
Camps, Pelayo; Iglesias, Carmen; Rodriguez, Maria Jesus; Grancha, Maria Desamparados; Gregori, Maria Eugenia; et al.
Chemische Berichte, 1988 , vol. 121, p. 647 - 654
参考文献
Camps, P.; Iglesias, C.; Lozano, R.; Miranda, M. A.; Rodriguez, M. J.
Tetrahedron Letters, 1987 , vol. 28, # 16 p. 1831 - 1832
反应条件
sodium hydroxide; sodium borohydride in methanol
参考文献
CALDERWOOD, DAVID; ARNOLD, LEE; MAZDIYASNI, HORMOZ; HIRST, GAVIN C.; DENG, BOJUAN B.; JOHNSTON, DAVID N.; RAFFERTY, PAUL; TOMETZKI, GERALD B.; TWIGGER, HELEN L.; MUNSCHAUER, RAINER
Patent: US2003/187001 A1, 2003 ;
US 20030187001 A1
反应条件
titanium tetrachloride; triethylamine 1) THF, 0-10 deg C, 2) 20-25 deg C, 36 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 125, # 4 p. 955 - 968
反应条件
n-butyllithium
Yield given. Multistep reaction;
参考文献
Eaton, Philip E.; Srikrishna, A.; Uggeri, Fulvio
Journal of Organic Chemistry, 1984 , vol. 49, # 10 p. 1728 - 1732
