5-(1-萘基)-2-糠醛合成路线 （共 4 条）
反应条件
potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0) in ethanol; water; toluene
Suzuki coupling; 5 h; Heating;
参考文献
Mitsch, Andreas; Wissner, Pia; Silber, Katrin; Haebel, Peter; Sattler, Isabel; Klebe, Gerhard; Schlitzer, Martin
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 17 p. 4585 - 4600
反应条件
bis-triphenylphosphine-palladium(II) chloride; lithium chloride in ethylene glycol dimethyl ether
T=60°C; Stille reaction; 1.5 h;
参考文献
Hosoya, Takamitsu; Aoyama, Hiroshi; Ikemoto, Takaaki; Kihara, Yasutaka; Hiramatsu, Toshiyuki; Endo, Makoto; Suzuki, Masaaki
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 5 p. 663 - 673
反应条件
potassium acetate; palladium diacetate in N,N-dimethyl acetamide
T=150°C; 20 h; Inert atmosphere;
参考文献
Dong, Jia Jia; Roger, Julien; Pogan, Franc; Doucet, Henri
Green Chemistry, 2009 , vol. 11, # 11 p. 1832 - 1846
反应条件
hydrogenchloride; sodium hydrogencarbonate; sodium nitrite
1) acetone, water, -10 to -5 deg C; 2) 30 to 40 deg C; Yield given. Multistep reaction;
参考文献
Obushak, N. D.; Lesyuk, A. I.; Ganushchak, N. I.; Mel'nik, G. M.; Zavalii, P. Yu.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 11 p. 2093 - 2097
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 11 p. 2331 - 2336
