1,4-二苄氧基-2-硝基苯合成路线 （共 6 条）
反应条件
1: With AlCl3, aluminium chloride in chloroform
T=0°C; 0.5 h;
2: With hydrogenchloride; water in chloroform
T=20°C; regioselective reaction;
参考文献
Ji, Xiujie; Cheng, Bowen; Song, Jun; Liu, Chao; Wang, Yufei
Synthetic Communications, 2009 , vol. 39, # 11 p. 2053 - 2057
反应条件
nitric acid in acetic acid
T=30°C; 0.5 h;
参考文献
Link, Helmut; Bernauer, Karl; Englert, Gerhard
Helvetica Chimica Acta, 1982 , vol. 65, # 8 p. 2645 - 2667
反应条件
1: alcoholic KOH-solution
2: concentrated nitric acid
View Scheme
参考文献
Schiff; Pellizzari
Justus Liebigs Annalen der Chemie, 1883 , vol. 221, p. 369
反应条件
1: potassium hydroxide / ethanol / 12 h / 20 °C
2: nitric acid / acetic acid / 12 h / 50 °C / |Cooling with ice
View Scheme
参考文献
Takei, Yoshiaki; Murata, Atsushi; Yamagishi, Kento; Arai, Satoshi; Nakamura, Hideki; Inoue, Takafumi; Takeoka, Shinji
Chemical Communications, 2013 , vol. 49, # 66 p. 7313 - 7315
反应条件
1: alcoholic KOH-solution
2: concentrated nitric acid
View Scheme
参考文献
Schiff; Pellizzari
Justus Liebigs Annalen der Chemie, 1883 , vol. 221, p. 369
反应条件
hydrogen; nickel in ethyl acetate
T=23°C; P=75.006 Torr; 3 h;
参考文献
Link, Helmut; Bernauer, Karl; Englert, Gerhard
Helvetica Chimica Acta, 1982 , vol. 65, # 8 p. 2645 - 2667
